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Study on Purification Diatomite with nitric acid by Thermal Closed System

机译:热密闭系统硝酸提纯硅藻土的研究。

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摘要

In this research, a purification approach using nitric acid leaching at thermal closed system was developed to improve the porous structure of raw diatomite by removal of impurities from its surface and clogged pores. The feasibility and efficiency of this approach were determined by XRF for chemical constitution of diatomite, SEM for morphology and BET for specific surface area of purified diatomite. The investigations indicated that the content of SiO2 was in order of 85.14% for raw diatomite and 98% for purified diatomite, the content of Fe2O3 decreases after purified; the integrity of the porous structure was confirmed by SEM, and increase in specific surface area from 18m2·g-1 to 36m2·g-1.Key words: thermal closed system / diatomite / low temperature / purification
机译:在这项研究中,开发了一种在热密闭系统中使用硝酸浸提的纯化方法,以通过从硅藻土表面除去杂质和堵塞孔眼来改善硅藻土原料的多孔结构。用XRF确定硅藻土的化学组成,用SEM测定形态,用BET测定纯化的硅藻土的比表面积,确定了该方法的可行性和有效性。研究表明,粗硅藻土的SiO2含量约为85.14%,纯硅藻土的含量​​为98%,纯化后Fe2O3的含量降低。 SEM证实了多孔结构的完整性,比表面积从18m2·g-1增加到36m2·g-1。关键词:热封闭系统/硅藻土/低温/净化

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