The High Surface Ratio Micro-MoS&sub&2&/sub& Grain Composed of MoS&sub&2&/sub& Nanosheet Prepared with One-Step Hydrothermal Synthesis

摘要

Micro molybdenum disulfide was prepared with one-step hydrothermal method; the influence of reactant concentration and temperature on the surface ratio of micro-MoS_(2) grain was investigated. Raman spectroscopy (Raman), X-ray diffraction (XRD), and Scanning electron microscopy (SEM) were used to characterize the structure, composition and morphology of MoS_(2). The results show that micro-MoS_(2) grains were synthesized with one-step hydrothermal synthesis, and the morphology of micro-MoS_(2) grains is like flower and sphere. The SEM figures indicate that the surface ratio of micro-MoS_(2) grains is different and also show that the surface ratio of micro-MoS_(2) grains can be improved by regulating reactant concentration and temperature. This research showed a method to improve the surface ratio of micro-MoS_(2) grains.