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Determining Contact Angle and Surface Energy of Co60Fe20B20Thin Films by Magnetron Sputtering

机译:磁控溅射测定Co60Fe20B20薄膜的接触角和表面能

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This study examined the deposition of CoFeB thin films on a glass substrate at room temperature (RT), as well as the effects of conducting postannealing at heat annealingTA=150°C for 1 h. The thickness (tf) of the CoFeB thin films ranged from 100 Å to 500 Å. The microstructure, average contact angle, and surface energy properties were also investigated. X-ray diffraction (XRD) revealed that CoFeB films are nanocrystalline at RT and that post-annealing treatment increases in conjunction with the crystallinity. The surface energy of the CoFeB thin films is related to adhesive strength. The CoFeB films form a contact angle of larger than90∘with water as a test liquid. This finding demonstrates that the CoFeB film is hydrophobic. Astfincreases from 100 Å to 500 Å, the surface energy at RT decreases from 40 mJ/mm2to 32 mJ/mm2. During post-annealing treatment, the surface energy increases from 32 mJ/mm2to 35 mJ/mm2, astfincreases from 100 Å to 300 Å; then it decreases to 31 mJ/mm2, astfincreases from 300 Å to 500 Å. The surface energy of the as-deposited CoFeB thin films exceeds that during post-annealing treatment at thicknesses of 100 Å and 200 Å, suggesting that as-deposited CoFeB thin film increases the adhesion.
机译:这项研究研究了在室温(RT)下在玻璃基板上CoFeB薄膜的沉积,以及在TA = 150°C的热退火条件下进行1?h后退火的影响。 CoFeB薄膜的厚度(tf)在100至500之间。还研究了微观结构,平均接触角和表面能性质。 X射线衍射(XRD)显示,CoFeB薄膜在室温下为纳米晶体,退火后处理随结晶度的增加而增加。 CoFeB薄膜的表面能与粘合强度有关。 CoFeB薄膜与水作为测试液体的接触角大于90°。该发现表明CoFeB膜是疏水的。弹性从100µA增加到500µÅ,RT的表面能从40µmJ / mm2降低到32µmJ / mm2。在退火后处理中,表面能从32 mJ / mm2增加到35 mJ / mm2,从100fromÅ增加到300Å;然后降低到31 mJ / mm2,从300Å上升到500Å。沉积后的CoFeB薄膜的表面能在厚度为100Å和200Å的情况下超过了退火后的表面能,这表明沉积后的CoFeB薄膜提高了附着力。

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