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首页> 外文期刊>Der chemica Sinica >Synthesis and Characterization of Assorted Heterocycles Based 3-(9Hcarbazol-9-yl) Propane Hydrazide
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Synthesis and Characterization of Assorted Heterocycles Based 3-(9Hcarbazol-9-yl) Propane Hydrazide

机译:基于3-(9Hcarbazol-9-yl)丙烷肼的各种杂环的合成与表征

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Efficient methodology for the synthesis of unrecorded series of heterocycles based carbazole sub-structure is reported. Carbazole heterocycles have been synthesized by employing 3-(9H-carbazol-9-yl)propanoic acid 1 as starting material. The precursor 3-(9H-carbazol-9-yl)propanehydrazide 3 was synthesized by reaction of ethyl 3-(9Hcarbazol- 9-yl)propanoate 2 with hydrazine hydrate in ethanol. The structures of synthesized compounds were confirmed on the basis of their elemental analysis and spectral results (IR, 1H and 13C NMR).
机译:报道了合成基于杂环的咔唑亚结构的未记录系列的有效方法。通过使用3-(9H-咔唑-9-基)丙酸1作为起始原料合成咔唑杂环。通过使3-(9H咔唑-9-基)丙酸乙酯2与水合肼在乙醇中反应来合成前体3-(9H-咔唑-9-基)丙酰肼3。根据其元素分析和光谱结果(IR,1H和13C NMR)确定合成化合物的结构。

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