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Preparation and Characterization of Copper Oxide Nanoparticles Synthesized via Chemical Precipitation Method

机译:化学沉淀法合成氧化铜纳米粒子的制备与表征

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Copper oxide nanoparticles (CuO-NPs) were synthesized via chemical precipitation method using copper (II) chloride dihydrate and sodium hydroxide. Then nanoparticles were characterized by using X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), Energy Dispersive X-ray (EDX), and Fourier Transform Infra Red (FTIR) spectroscopy. The XRD patterns and EDX spectra showed that the prepared CuO-NPs were highly pure, crystalline and nano-sized. The SEM image suggested that nano particles were spherical and there was a tendency of agglomerations. The nanoparticles showed interactions between copper and oxygen atoms supported by FTIR studies.
机译:采用二水合氯化铜(II)和氢氧化钠通过化学沉淀法合成了氧化铜纳米颗粒(CuO-NPs)。然后通过使用X射线衍射(XRD),扫描电子显微镜(SEM),能量色散X射线(EDX)和傅立叶变换红外(FTIR)光谱对纳米颗粒进行表征。 XRD图谱和EDX光谱表明,所制备的CuO-NP具有较高的纯度,结晶度和纳米级。 SEM图像表明纳米颗粒是球形的并且有团聚的趋势。 FTIR研究表明,纳米粒子显示出铜和氧原子之间的相互作用。

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