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Preparation and Characterization of Cerium (III) Doped Captopril Nanoparticles and Study of their Photoluminescence Properties

机译:铈(III)掺杂卡托普利纳米颗粒的制备,表征及光致发光性能研究

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In this research Ce3+ doped Captopril nanoparticles (Ce3+ doped CAP-NP) were prepared by a cold welding process and have been studied. Captopril may be applied in the treatment of hypertension and some types of congestive heart failure and for preventing kidney failure due to high blood pressure and diabetes. CAP-NP was synthesized by a cold welding process. The cerium nitrate was added at a ratio of 10% and the optical properties have been studied by photoluminescence (PL). The synthesized compounds were characterized by Fourier transform infrared spectroscopy. The size of CAP-NP was calculated by X-ray diffraction (XRD). The size of CAP-NP was in the range of 50 nm. Morphology of surface of synthesized nanoparticles was studied by scanning electron microscopy (SEM). Finally the luminescence properties of undoped and doped CAP-NP were compared. PL spectra from undoped CAP-NP show a strong pack in the range of 546 nm after doped cerium ion into the captopril appeared two bands at 680 and 357 nm, which is ascribed to the well-known 5d–4f emission band of the cerium.
机译:在这项研究中,通过冷焊工艺制备了Ce3 +掺杂的Captopril纳米颗粒(Ce3 +掺杂的CAP-NP)并进行了研究。卡托普利可用于治疗高血压和某些类型的充血性心力衰竭,以及预防由于高血压和糖尿病引起的肾衰竭。 CAP-NP是通过冷焊工艺合成的。以10%的比例添加硝酸铈,并且已经通过光致发光(PL)研究了光学性质。通过傅立叶变换红外光谱对合成的化合物进行表征。通过X射线衍射(XRD)计算CAP-NP的大小。 CAP-NP的大小在50nm的范围内。通过扫描电子显微镜(SEM)研究了合成纳米颗粒的表面形态。最后比较了未掺杂和掺杂的CAP-NP的发光特性。来自未掺杂的CAP-NP的PL光谱显示,在掺杂到卡托普利中的铈离子在680和357 nm处出现两个谱带后,在546 nm范围内有一个很强的堆积,这归因于众所周知的铈5d–4f发射谱带。

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