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Influence of polymerization cycle in properties of acrylic resin polymerized by microwave energy

机译:聚合周期对微波能聚合丙烯酸树脂性能的影响

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Objective: The purpose of this study was to evaluate the physicochemical properties of acrylic resin?polymerized by microwave energy in short cycle of polymerization. Methods: Two brands (Classico and VIPI) and two cycles were evaluated (manufacturer cycle and?short cycle). The characteristics and properties as degree of conversion, glass transition temperature,?impact strength-Izod, Knoop hardness, swelling degree, soluble fraction, specific mass, water?sorption and solubility were evaluated. Results: Glass transition temperature, hardness, specific mass, soluble fraction and solubility were?statistically significant between cycles and brands (p0.05). Water sorption showed no difference?between cycles (p0.05) and impact strength presented difference between brands in short cycle?(p0.05). Acrylic resin polymerized by microwave energy with manufacturer cycle presented no?difference in physicochemical properties between evaluated brands.?Conclusion: The short cycle of polymerization showed reduced properties in microwave acrylic?resin when compared to manufacturer cycle. Manufacturer cycle of polymerization should be used?to acrylic resin devices production.
机译:目的:本研究的目的是评估在短周期聚合中由微波能量聚合的丙烯酸树脂的理化性质。方法:对两个品牌(Classico和VIPI)和两个周期进行了评估(制造商周期和短周期)。评价了转化率,玻璃化转变温度,冲击强度-艾佐德(Izod),努氏硬度,溶胀度,可溶性分数,比重,吸水率和溶解度的特性和性质。结果:玻璃化转变温度,硬度,比质量,可溶分数和溶解度在各周期和各品牌之间具有统计学意义(p <0.05)。循环之间的吸水率无差异(p> 0.05),短循环中各品牌之间的冲击强度差异也有差异(p <0.05)。通过微波能量与制造商循环聚合的丙烯酸树脂在所评估品牌之间的理化性能没有差异。结论:与制造商循环相比,聚合的短循环显示微波丙烯酸树脂的性能下降。制造商应使用聚合反应周期进行丙烯酸树脂装置的生产。

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