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首页> 外文期刊>Research Journal of Chemical Sciences >Production of Activated Carbon from Sugarcane Bagasse by Chemical Activation with ZnCl2: Preparation and Characterization Study
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Production of Activated Carbon from Sugarcane Bagasse by Chemical Activation with ZnCl2: Preparation and Characterization Study

机译:ZnCl2活化甘蔗渣制活性炭的制备与表征研究

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A protocol producing the activated carbon (AC) with high surface area and porosity with large adsorption capacity from non-toxic and low cost precursor source was developed. The ACwas prepared from sugarcane bagasse with ZnCl2as activating agent. Three preparing temperatures including 400oC, 500oC, and 600oC were investigated to compare the structural difference of the ACs. The properties of the ACsfabricated at these temperatures were determined using relevant techniques such as scanning electron microscopy (SEM), X-ray diffraction (XRD), thermo-gravimetric analysis (TGA),Fourier transform infrared (FT-IR) spectroscopy and nitrogen adsorption/desorptionmeasurement.Characterization results showed that the maximum BET surface area of the AC is1502.1 m2/g at 500oC. XRD patternsand SEM micrographs revealed that the ACshave the amorphous structure and heterogeneous surface. IR spectra also proved the presence of functional groups O-H, O-N asymmetric and C-C aromatic in the carbon. Moreover, the maximum AC yield of 45.7% was achieved at 500oC.
机译:制定了从无毒且成本低廉的前体来源生产具有高表面积和孔隙率,大吸附能力的活性炭(AC)的方案。 AC是用甘蔗渣和ZnCl2作为活化剂制备的。研究了三种制备温度,包括400oC,500oC和600oC,以比较AC的结构差异。使用诸如扫描电子显微镜(SEM),X射线衍射(XRD),热重分析(TGA),傅立叶变换红外(FT-IR)光谱和氮吸附等相关技术确定在这些温度下制造的AC的性能表征结果表明,在500oC下,AC的最大BET表面积为1502.1 m2 / g。 XRD图谱和SEM照片表明,AC具有非晶结构和异质表面。红外光谱还证明碳中存在官能团O-H,O-N不对称和C-C芳香族。此外,在500oC时,最大AC产量达到45.7%。

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