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Evaluation of linear polymerization shrinkage, flexural strength and modulus of elasticity of dental composites

机译:牙科复合材料的线性聚合收缩率,弯曲强度和弹性模量评估

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Linear polymerization shrinkage (LPS), flexural strength (FS) and modulus of elasticity (ME) of 7 dental composites (Filtek Z350™, Filtek Z250™/3M ESPE; Grandio™, Polofil Supra™/VOCO; TPH Spectrum™, TPH3™, Esthet-X™/Denstply) were measured. For the measurement of LPS, composites were applied to a cylindrical metallic mold and polymerized (n = 8). The gap formed at the resin/mold interface was observed using scanning electron microscopy (1500×). For FS and ME, specimens were prepared according to the ISO 4049 specifications (n = 10). Statistical analysis of the data was performed with one-way ANOVA and the Tukey test. TPH Spectrum presented significantly higher LPS values (29.45 μm). Grandio had significantly higher mean values for FS (141.07 MPa) and ME (13.91 GPa). The relationship between modulus of elasticity and polymerization shrinkage is the main challenge for maintenance of the adhesive interface, thus composites presenting high shrinkage values, associated with a high modulus of elasticity tend to disrupt the adhesive interface under polymerization.
机译:7种牙科复合材料(Filtek Z350™,Filtek Z250™/ 3M ESPE; Grandio™,Polofil Supra™/ VOCO; TPH Spectrum™,TPH3™)的线性聚合收缩率(LPS),挠曲强度(FS)和弹性模量(ME) (Esthet-X TM / Denstply)。为了测量LPS,将复合材料施加到圆柱形金属模具上并聚合(n = 8)。使用扫描电子显微镜(1500x)观察在树脂/模具界面处形成的间隙。对于FS和ME,根据ISO 4049规范(n = 10)制备样品。使用单向方差分析和Tukey检验对数据进行统计分析。 TPH光谱显示LPS值明显更高(29.45μm)。 Grandio的FS(141.07 MPa)和ME(13.91 GPa)的平均值明显更高。弹性模量与聚合收缩率之间的关系是维持粘合剂界面的主要挑战,因此呈现出高收缩率的复合材料与高弹性模量相关联,往往会破坏聚合反应下的粘合剂界面。

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