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Rapid Alloy Development of Extremely High-Alloyed Metals Using Powder Blends in Laser Powder Bed Fusion

机译:在激光粉末床熔合中使用粉末混合物快速发展极高合金金属的合金

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The design of new alloys by and for metal additive manufacturing (AM) is an emerging field of research. Currently, pre-alloyed powders are used in metal AM, which are expensive and inflexible in terms of varying chemical composition. The present study describes the adaption of rapid alloy development in laser powder bed fusion (LPBF) by using elemental powder blends. This enables an agile and resource-efficient approach to designing and screening new alloys through fast generation of alloys with varying chemical compositions. This method was evaluated on the new and chemically complex materials group of multi-principal element alloys (MPEAs), also known as high-entropy alloys (HEAs). MPEAs constitute ideal candidates for the introduced methodology due to the large space for possible alloys. First, process parameters for LPBF with powder blends containing at least five different elemental powders were developed. Secondly, the influence of processing parameters and the resulting energy density input on the homogeneity of the manufactured parts were investigated. Microstructural characterization was carried out by optical microscopy, electron backscatter diffraction (EBSD), and energy-dispersive X-ray spectroscopy (EDS), while mechanical properties were evaluated using tensile testing. Finally, the applicability of powder blends in LPBF was demonstrated through the manufacture of geometrically complex lattice structures with energy absorption functionality.
机译:金属增材制造(AM)以及用于金属增材制造(AM)的新合金设计是一个新兴的研究领域。当前,预合金粉末用于金属增材制造中,就化学成分的变化而言,它们价格昂贵且不灵活。本研究描述了通过使用元素粉末混合物在激光粉末床熔合(LPBF)中快速合金发展的适应性。这样可以通过快速生成具有不同化学成分的合金来设计和筛选新合金的灵活,资源高效的方法。对该方法进行了评估,该方法基于化学成分复杂的新型多元素元素合金(MPEA),也称为高熵合金(HEA)。由于可能的合金空间很大,MPEA构成了引入方法的理想候选者。首先,开发了包含至少五种不同元素粉末的粉末混合物的LPBF的工艺参数。其次,研究了加工参数和输入的能量密度输入对所制造零件均质性的影响。通过光学显微镜,电子背散射衍射(EBSD)和能量色散X射线光谱(EDS)进行微观结构表征,同时使用拉伸试验评估机械性能。最后,通过制造具有能量吸收功能的几何复杂晶格结构,证明了粉末共混物在LPBF中的适用性。

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