One-pot solid phase selective aromatization of cholesterol using N-bromosuccinimide: an optimized green methodology

Pranab Ghosh; Jayanta Das; Antara Sarkar

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One-pot solid phase selective aromatization of cholesterol using N-bromosuccinimide: an optimized green methodology

机译：使用N-溴代琥珀酰亚胺对胆固醇进行一锅固相选择性芳香化：一种优化的绿色方法

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摘要

One-pot silica promoted selective aromatization of ring-A of cholesterol using N-bromosuccinimide (NBS) has been performed. The structure of the compound has been characterized by spectral analysis (UV, FT-IR, NMR, and Mass).

机译：已经进行了使用N-溴琥珀酰亚胺（NBS）的一锅法二氧化硅促进胆固醇的A环选择性芳香化。该化合物的结构已通过光谱分析（UV，FT-IR，NMR和质量）进行了表征。

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《Green Chemistry Letters and Reviews 》 |2012年第2期| 共5页
作者
Pranab Ghosh; Jayanta Das; Antara Sarkar;
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中图分类化学 ;
关键词
cholesterolaromatizationN-bromosuccinimide;

机译：胆固醇芳香化N-溴琥珀酰亚胺;

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1. One-pot solid phase selective aromatization of cholesterol using N-bromosuccinimide: an optimized green methodology [J] . Pranab Ghosha* Jayanta Dasa Antara Sarkara Green Chemistry Letters and Reviews . 2012 ,第2期

机译：使用N-溴代琥珀酰亚胺对胆固醇进行一锅固相选择性芳香化：一种优化的绿色方法
2. Solid phase selective oxidation of beta-sitosterol and 4 beta-hydroxy cholesterol by N-bromosuccinhnide - A green approach [J] . Ghosh Pranab, Sarkar Antara, Das Jayanta Journal of the Indian Chemical Society . 2014 ,第12期

机译：N-溴代琥珀酰亚胺固相选择性氧化β-谷甾醇和4个β-羟基胆固醇-一种绿色方法
3. Selectivity optimization in green chromatography by gradient stationary phase optimized selectivity liquid chromatography [J] . Chen K., Lynen F., De Beer M., Journal of chromatography, A: Including electrophoresis and other separation methods . 2010 ,第46期

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4. Optimization of subcritical 1, 1,1, 2-tetrafluoroethane ( R134a ) removal of cholesterol from spray-dried Sthenoteuthis oualaniensis egg powder using response surface methodology [C] . Xiao Sui, Xiaomei Feng, Rongyan Yue International Conference on Chemical Engineering and Advanced Materials . 2014

机译：利用响应面方法从喷雾干燥的斯坦托纳斯Oualaniensis蛋粉中除去亚临界1,1,1,2-四氟乙烷（R134A）的优化使用响应表面方法
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. Peptide fragmentation suitable for solid-phase microsequencing. Use of N-bromosuccinimide and BNPS-skatole (3-bromo-3-methyl-2-(2-nitrophenyl)thio-3H-indole). [O] . P E Hunziker, G J Hughes, K J Wilson 1980

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7. Selectivity Control in the Tandem Aromatization of Bio-Based Furanics Catalyzed by Solid Acids and Palladium [O] . Genuino, Homer C, Thiyagarajan, Shanmugam, van der Waal, Jan C, 2016

机译：固体酸和钯催化生物基呋喃的串联芳构化选择性控制
8. UNEP greenhouse gas abatement costing studies. Phase two. Analysis of abatement costing issues and preparation of a methodology to undertake national greenhouse gas abatement costing studies. Part 2: Country summaries [R] . 1994

机译：联合国环境规划署温室气体减排成本研究。第二阶段。分析减排成本问题和准备进行国家温室气体减排成本研究的方法。第2部分：国家摘要

One-pot solid phase selective aromatization of cholesterol using N-bromosuccinimide: an optimized green methodology

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