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Fabrication of Porous Hydroxyapatite through Combination of Sacrificial Template and Direct Foaming Techniques

机译:牺牲模板与直接发泡技术相结合制备多孔羟基磷灰石

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The porous hydroxyapatite (HA) bioceramics were prepared through combination of sacrificial template and direct foaming techniques using PMMA granules (varied from 5 to 50 wt% in content) as a template and H2O2 solution (varied from 5 to 30 wt% in concentration) as a foaming agent, respectively. The effects of PMMA content and H2O2 concentration on final porosity, microstructure and mechanical strengths were studied. The porous samples using PMMA provided the porosity ranging from 52% to 75%, the samples using H2O2 had the porosity ranging from 82% to 85%, and the sample using both pore formers provided the porosity ranging between 84% and 90%. The higher content of PMMA and concentration of H2O2 led the porosity increased, leading to a decrease in the compressive and flexural strengths. Furthermore, this combination technique allowed interconnected pores having two levels of pore size, which were come from PMMA and H2O2. The PMMA formed the small pores with the diameter ranging between 100 and 300 μm, while H2O2 provided the larger pores with the diameter ranging from 100 to 1,000 μm depending on concentration. (49 views)
机译:多孔羟基磷灰石(HA)生物陶瓷是通过牺牲模板和直接发泡技术相结合制备的,使用PMMA颗粒(含量在5至50 wt%之间)和H2O2溶液(浓度在5至30 wt%之间)作为模板。分别是发泡剂。研究了PMMA含量和H2O2浓度对最终孔隙率,微观结构和机械强度的影响。使用PMMA的多孔样品的孔隙率在52%到75%之间,使用H2O2的样品的孔隙率在82%到85%之间,使用两种成孔剂的样品的孔隙率在84%到90%之间。较高的PMMA含量和H2O2浓度导致孔隙率增加,导致抗压强度和抗弯强度降低。此外,这种组合技术允许互连的孔具有两个级别的孔径,这些孔径来自PMMA和H2O2。 PMMA形成了直径在100到300μm之间的小孔,而H2O2提供了直径在100到1,000μm之间的大孔,具体取决于浓度。 (49观看次数)

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