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首页> 外文期刊>International Journal of Electrochemical Science >Mechanical, Microstructural and Tribo-Electrochemistry Characterization in Aqueous Media of Coatings Vanadium / Vanadium Nitride Used as Functional Coating for Implants
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Mechanical, Microstructural and Tribo-Electrochemistry Characterization in Aqueous Media of Coatings Vanadium / Vanadium Nitride Used as Functional Coating for Implants

机译:涂层钒/氮化钒用作植入物功能涂层的水性介质中的机械,微结构和摩擦电化学特性

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The study presents tribo-electrochemistry properties of multilayers of Vanadium / vanadium nitride [V/ VN] n (n = 1, 20, 50 and 100) deposited on surgical grade steel 316LVM through the Physical VaporDeposition processes (PVD) using Magnetron Sputtering Technology. Nanoindentation tests wereperformed to determine the hardness of the coatings corrosion tests and assays tribocorrosion (synergybetween corrosion and wear), which were carried out with equipment potentiostatic type adapted to apin on disk tribometer also performed which was adapted to an electrochemical cell with threeelectrodes: A silver/silver chloride reference electrode (Ag/AgCl), a counter electrode of platinum anda working electrode immersed in a solution of ringers lactate at a temperature of 37 C. The evaluationof the tribo-corrosion testing was performed using the electrochemical technique potentiodynamiccurve to calculate the value of polarization resistance Tafel polarization curves to determine thecorrosion rate in the coatings. The characterization of microstructural and morphological subjected tofretting corrosion coatings it was performed using the technique of atomic force microscopy (AFM).
机译:这项研究提出了使用磁控溅射技术通过物理气相沉积工艺(PVD)沉积在手术级钢316LVM上的钒/氮化钒[V / VN] n(n = 1、20、50和100)多层膜的摩擦电化学性质。进行纳米压痕测试,以确定涂层的硬度。腐蚀测试和摩擦腐蚀(腐蚀与磨损之间的协同作用)试验,是用适合于固定在磁盘摩擦计上的恒电位型设备进行的,也适用于具有三电极的电化学电池:银/氯化银参比电极(Ag / AgCl),铂的对电极和浸入乳酸林格氏液中的工作电极,温度为37°C。使用电化学技术电位动力学曲线对摩擦腐蚀试验进行评估,以计算出极化电阻的值通过塔菲尔极化曲线确定涂层的腐蚀速率。使用原子力显微镜(AFM)技术对微蚀腐蚀涂层的微观结构和形态进行表征。

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