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Preparation and Characterization of Natural Zeolite and Rice Husk Ash as Filler Material HDPE Thermoplastic

机译:天然沸石和稻壳灰填充材料HDPE热塑性塑料的制备与表征

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This study aims to determine the size of the natural zeolite partike, rice husk ash, and to know the effect of fillers on the mechanical strength of the composite. The method is done by two methods, the first method of natural zeolite and rice husk ash puree by using Ball Mill for 1 hour to obtain a particle size of 74 μm. Further to the natural zeolite dissolved in 2 M HCl, rice husk ash with NaOH 2.5 M. results of each ingredient in a ball mill for 15 hours to obtain particles in nano-meter size. Both of these materials are used as filler in thermoplastic HDPE. This mixture of materials with a ratio (70/30, 60/40, 50/50, 40/60, 30/70) wt% were mixed in an internal mixer at a temperature of 150 0 C laboplastomil at a rate of 60 rpm for 10 minutes. The results of XRD analysis of rice husk ash obtained particle size of 53.12 nm with dominant phase of SiO 2 (Cristobalite). For natural zeolite obtained size 44.46 nm with dominant phase Al 2 CaO 8 Si 2 (Anorthite). mechanical properties of the composites, obtained the biggest increase in a mixture of 60/40 compared to pure HDPE.
机译:这项研究旨在确定天然沸石石粉,稻壳灰的尺寸,并了解填料对复合材料机械强度的影响。该方法通过两种方法完成,第一种方法是使用Ball Mill将天然沸石和稻壳灰原浆混合1小时,以获得74μm的粒径。除了将天然沸石溶解在2 M HCl中外,将稻壳灰分与NaOH 2.5 M混合,在球磨机中将每种成分研磨15小时,以获得纳米尺寸的颗粒。这两种材料都用作热塑性HDPE的填料。将比例为(70 / 30、60 / 40、50 / 50、40 / 60、30 / 70)wt%的这种材料混合物在内部混合器中在150 0 Claboplastomil温度下以60 rpm的速率混合10分钟。稻壳灰分的XRD分析结果表明,其主相为SiO 2(方石英),粒径为53.12 nm。对于天然沸石,获得的尺寸为44.46nm,且主相为Al 2 CaO 8 Si 2(钠钙铝石)。与纯HDPE相比,复合材料的机械性能在60/40的混合物中获得了最大的增长。

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