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Influence of chemical degradation and abrasion on surface properties of nanorestorative materials

机译:化学降解和磨损对纳米修复材料表面性能的影响

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Aim: The aim of this in vitro study was to investigate the synergistic effect of chemical degradation (erosion) and three-body abrasion (mechanical degradation) on the surface roughness (Ra) and hardness (KHN) of two nanorestorative materials and two conventional materials.Methods: Disc-shaped specimens (5 mm in diameter, 2 mm thick) of Filtek Z350TM and TPH SpectrumTM composites and Ketac NanoTM and VitremerTM light-curing glass ionomer cements, nanomaterials and conventional materials were prepared according to the manufacturer's instructions. After 24 h, polishing procedures were performed and initial measurements of Ra and KHN were taken in all specimens. The specimens were divided into 12 groups (n = 10) according to material and storage media: artificial saliva, orange juice, and Coca-Cola(r). After 30 days of storage, the specimens were submitted to mechanical degradation and re-evaluated for Ra and KHN. Data were tested for significant differences by repeated-measure three-way ANOVA and Tukey's tests (p0.05).Results: Erosion and abrasion wear significantly decreased hardness of all materials. Only Filtek Z350 roughness, however, was not affected by erosion and abrasion. All materials showed a significant increase in surface roughness after erosion and abrasion, except for Filtek Z350. After chemical and mechanical degradation, the KHN of all samples had decreased significantly. After mechanical degradation, the acidic drinks (Coca-Cola(r) and orange juice) were more aggressive than artificial saliva to all materials.Conclusions: A synergistic effect was observed by the increase in roughness for all materials, except for Filtek Z350; hardness values decrease for all materials, regardless of whether they were nanofilled or not. The RMGICs were more susceptible to degradation than the composites, considering both hardness and roughness surface parameters.
机译:目的:这项体外研究的目的是研究化学降解(侵蚀)和三体磨损(机械降解)对两种纳米修复材料和两种常规材料的表面粗糙度(Ra)和硬度(KHN)的协同作用。方法:Filtek Z350 TM 和TPH Spectrum TM 复合材料以及Ketac Nano TM 和Vitremer TM 光固化玻璃离聚物水泥,纳米材料和常规材料均根据制造商的说明进行制备。 24小时后,进行抛光程序,并对所有样品进行Ra和KHN的初始测量。根据材料和存储介质将样品分为12组(n = 10):人造唾液,橙汁和可口可乐。储存30天后,将样品进行机械降解,并重新评估Ra和KHN。通过重复测量三向ANOVA和Tukey检验来检验数据的显着差异(p <0.05)。结果:侵蚀和磨损明显降低了所有材料的硬度。但是,只有Filtek Z350粗糙度不受腐蚀和磨损的影响。除Filtek Z350外,所有材料在腐蚀和磨蚀后的表面粗糙度均显着增加。经过化学和机械降解后,所有样品的KHN均显着降低。机械降解之后,酸性饮料(可口可乐和橙汁)对所有材料的侵蚀性都比人工唾液强。结论:除Filtek Z350外,所有材料的粗糙度均增加了协同作用。所有材料的硬度值都会降低,无论它们是否被纳米填充。考虑到硬度和粗糙度表面参数,RMGIC比复合材料更容易降解。

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