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Influence of radiant exposure on contraction stress, degree of conversion and mechanical properties of resin composites

机译:辐射暴露对树脂复合材料收缩应力,转化度和力学性能的影响

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Objective. To verify the influence of radiant exposure (H) on contraction stress (CS), degree of conversion (DC) and mechanical properties of two restorative composites. Methods. Filtek Z250 (3M ESPE) and Heliomolar (Ivoclar) were photoactivated with 6,12, 24, or 36J/cm~2 at continuous irradiance of 600mW/cm~2. CS at 10min was determined in a low compliance testing system. DC, flexural strength (FS), flexural modulus (FM) and Knoop microhardness (KHN) were measured after 24h storage at 37℃. KHN and DC measurements were conducted on the irradiated surface of 1 mm thick disk-shaped specimens. Bar-shaped specimens were submitted to three-point bending to determine FS and FM. Data were analyzed by one-way ANOVA/Tukey's test (α = 0.05) separately for each composite. Results. For Filtek Z250, no significant increase in CS was observed above 12J/cm~2. DC and FM were similar at all H values, while FS increased significantly between 6 and 24J/cm~2. KHN was significantly different among all H levels, except between 12 and 24J/cm~2. For Heliomolar, CS and KHN increased significantly with H, except between 24 and 36 J/cm~2. DC, FM and FS did not vary, regardless of the radiant exposure. Significance. Variables tested behaved differently. CS and KHN were more sensitive to increasing radiant exposures than the other properties evaluated. FS varied only for Filtek Z250, while, for both composites, DC and FM were not affected by different H values.
机译:目的。为了验证辐射暴露(H)对收缩应力(CS),转化度(DC)和两种修复性复合材料的机械性能的影响。方法。 Filtek Z250(3M ESPE)和Heliomolar(Ivoclar)在连续照射600mW / cm〜2的条件下分别以6,12、24或36J / cm〜2光活化。在低一致性测试系统中确定了10分钟时的CS。在37℃下储存24小时后,测量DC,弯曲强度(FS),弯曲模量(FM)和努氏显微硬度(KHN)。 KHN和DC测量是在1毫米厚的圆盘状样品的辐照表面上进行的。将棒状样品进行三点弯曲以确定FS和FM。对于每种复合材料,分别通过单因素方差分析/ Tukey检验(α= 0.05)分析数据。结果。对于Filtek Z250,高于12J / cm〜2时CS值没有显着增加。在所有H值下DC和FM都相似,而FS在6至24J / cm〜2之间显着增加。除12至24J / cm〜2外,KHN在所有H水平之间均存在显着差异。对于Heliomolar,CS和KHN随H显着增加,除了在24至36 J / cm〜2之间。不论辐射量如何,DC,FM和FS均没有变化。意义。测试的变量表现不同。 CS和KHN对辐射暴露的增加比所评估的其他特性更为敏感。 FS仅对于Filtek Z250有所不同,而对于两种复合材料,DC和FM均不受不同H值的影响。

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