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The effect of ceramic and porous fillers on the mechanical properties of experimental dental composites

机译:陶瓷和多孔填料对牙科复合材料力学性能的影响

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Objectives. The purpose of this study was to investigate the effect of ceramic fillers (containing leucite crystals) and their porosity on the mechanical properties of a new experimental dental composite in order to compare with the properties of composites containing conventional glass fillers. Methods. In this study, experimental composites were prepared by mixing the silane-treated fillers with monomers. Experimental composites were divided into four groups according to their filler type, amount and porosity. The monomers were composed of 70% Bis-GAAA and 30% TEGDMA by weight for all groups. Glass and leucite-containing-ceramic were prepared as different filler types. In order to make fillers porous, leucite-containing-ceramic fillers were treated with HF acid. Camphorquinone and DMAEMA were used as photo initiator system. Post-curing was done for all groups before mechanical testing. Degree of Conversion of composites was measured using FTIR spectroscopy. The diametral tensile strength (DTS), flexural strength and flexural modulus were measured and compared among the groups. Results. The results showed that the stronger and more porous filler has a positive effect on flexural strength. Porosity of filler increased flexural strength significantly. No significant difference was found in DTS tests among the groups. Flexural modulus was affected and increased by using ceramic fillers. The type of the filler affected the DC of the composite and DC increased by post-curing. Significance: Flexural strength is one of the most important properties of restorative dental materials. Higher flexural strength can be achieved by stronger and more porous fillers. Investigation into the effect of filler on dental material properties would be beneficial in the development of restorative dental material.
机译:目标。这项研究的目的是研究陶瓷填料(含有白榴石晶体)及其孔隙率对新型实验牙科复合材料的机械性能的影响,以便与含有常规玻璃填料的复合材料的性能进行比较。方法。在这项研究中,通过将硅烷处理的填料与单体混合来制备实验复合材料。实验性复合材料根据其填料类型,用量和孔隙率分为四类。对于所有组,单体由70重量%的Bis-GAAA和30重量%的TEGDMA组成。制备玻璃和含白晶的陶瓷作为不同的填料类型。为了使填料多孔,用HF酸处理含白沸石的陶瓷填料。樟脑醌和DMAEMA被用作光引发剂系统。在机械测试之前,对所有组都进行了后固化。使用FTIR光谱法测量复合材料的转化度。测量并比较各组的径向拉伸强度(DTS),弯曲强度和弯曲模量。结果。结果表明,更坚固,更多孔的填料对弯曲强度有积极影响。填料的孔隙率显着提高了挠曲强度。各组之间在DTS测试中没有发现显着差异。通过使用陶瓷填料,弯曲模量受到影响并增加。填料的类型会影响复合材料的DC,而后固化会增加DC。启示:抗弯强度是修复性牙科材料的最重要特性之一。较高的抗弯强度可以通过使用强度更高且多孔的填料来实现。研究填料对牙科材料性能的影响将有利于开发修复性牙科材料。

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