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Identification of failure mechanisms of metallised glass fibre reinforced composites under tensile loading using acoustic emission analysis

机译:利用声发射分析识别金属化玻璃纤维增​​强复合材料在拉伸载荷下的破坏机理

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摘要

In this work, failure mechanisms of metallised glass fibre reinforced epoxy composites under tensile loading were investigated using acoustic emission analysis. Sandblasting with Al2O3 was used to pre-treat the composite surface prior to metallisation, and therefore to improve adhesion. The sandblasting time was varied from 2 s to 6 s. A two-step metallisation process consisting of electroless and subsequent electroplating was used for depositing the copper coating on the pre-treated composite surface. The mechanical pre-treatment had no significant negative effect on the mechanical properties of the composite laminate. The acoustic emission (AE) from the metallised composite was recorded during tensile testing in order to investigate the failure mechanisms. AE-Signals were analysed using pattern recognition and frequency analysis techniques. A correlation between the cumulative absolute AE-energy and the mechanical behaviour of uncoated and coated specimens during tensile testing was successfully observed. It was shown that a stronger adhesion between substrate and coating leads to a lower release of mechanical elastic energy, which could be recorded by means of AE analysis. Furthermore, differences in peak frequency, frequency distribution and the use of pattern recognition techniques allowed classifying the signal into three failure mechanisms for the uncoated samples and four failure mechanisms for the coated samples, namely matrix cracking, fibre-matrix interface failure, fibre breakage and substrate-coating interface failure. Waveform and frequency analysis of the classified signals supported the identification of the failure mechanisms. Furthermore, optical investigation and SEM images of the tested samples and fracture surfaces confirmed the identified mechanisms evaluated by acoustic emission analysis. (C) 2015 Elsevier Ltd. All rights reserved.
机译:在这项工作中,使用声发射分析研究了金属化玻璃纤维增​​强环氧复合材料在拉伸载荷下的破坏机理。在金属化之前,用Al2O3喷砂处理了复合材料表面,从而提高了附着力。喷砂时间从2秒到6秒不等。使用由无电镀和后续电镀组成的两步​​金属化工艺,将铜涂层沉积在预处理的复合材料表面上。机械预处理对复合层压板的机械性能没有明显的负面影响。在拉伸测试过程中记录了金属化复合材料的声发射(AE),以研究破坏机理。使用模式识别和频率分析技术对AE信号进行了分析。成功地观察到了累积绝对AE能量与拉伸试验过程中未涂层和涂层样品的机械性能之间的相关性。结果表明,基材与涂层之间更强的粘附力导致较低的机械弹性能释放,这可以通过AE分析来记录。此外,峰值频率,频率分布和模式识别技术的使用差异使信号可以分为未涂层样品的三种失效机理和涂层样品的四种失效机理,即基质破裂,纤维-基质界面失效,纤维断裂和基材涂层界面故障。分类信号的波形和频率分析支持故障机理的识别。此外,测试样品和断裂表面的光学研究和SEM图像证实了通过声发射分析评估的确定机理。 (C)2015 Elsevier Ltd.保留所有权利。

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