In-situ TiB/Ti-6Al-4V composites with a tailored architecture produced by hot isostatic pressing: Microstructure evolution, enhanced tensile properties and strengthening mechanisms

摘要

In-situ synthesized titanium borides reinforced Ti-6Al-4V composites with a tailored reinforcement architecture were successfully prepared by hot isostatic pressing (HIP) starting from a TiB2/Ti-6Al-4V powder system. The microstructure of the composite samples was investigated using X-ray diffraction (XRD) technique and scanning electron microscopy (SEM), and the mechanical properties were evaluated through room and high temperature tensile testing. It is found that during HIP the additive particles TiB2 have totally transformed into TiB needles, which tend to decorate at prior particle boundaries of the consolidated powder particles to form a network structure. With increasing TiB2 addition from 3 wt.% to 8 wt.%, the microstructural feature of the TiB network structure experiences the variations of discontinuous TiB reinforcement - quasi-continuous TiB reinforcement - continuous TiB reinforcement. The room temperature tensile properties of the composites are improved with increasing addition of TiB2 from 3 wt.% to 5 wt.%, but the tensile strength of the sample with 8 wt.% TiB2 drastically decreases. As to the high temperature properties, the titanium boride reinforced Ti-6Al-4V alloy composites can be an increased maximum service temperature by over 200 degrees C while retaining the same tensile strength accompanied with a suitable elongation. The strengthening mechanism is mainly attributed to the load-bearing transformation, grain refinement and dispersion strengthening.