The template effect of solvents on high yield synthesis, co-cyclization of pillar[6]arenes and interconversion between pillar [5]- and pillar[6]arenes

Tomoki Ogoshi; Naosuke Ueshima; Tomohiro Akutsu; Daiki Yamafuji; Takuya Furuta; Fumiyasu Sakakibara; Tada-aki Yamagishi

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The template effect of solvents on high yield synthesis, co-cyclization of pillar[6]arenes and interconversion between pillar [5]- and pillar[6]arenes

机译：溶剂的模板作用对高产合成，柱[6]芳烃的共环化以及柱[5]-和柱[6]芳烃之间的相互转化

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摘要

We have synthesized a pillar[6]arene in high yield and a co-pillar[6]arene using chlorocyclohexane as a solvent.

机译：我们以氯环己烷为溶剂，以高收率合成了支柱[6]芳烃和共立柱[6]芳烃。

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来源
《Chemical Communications》 |2014年第43期|5774-5777|共4页
作者
Tomoki Ogoshi; Naosuke Ueshima; Tomohiro Akutsu; Daiki Yamafuji; Takuya Furuta; Fumiyasu Sakakibara; Tada-aki Yamagishi;
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Graduate School of Natural Science and Technology, Kanazawa University, Kakuma-machi, Kanazawa, 920-1192, Japan,JST, PRESTO, 4-1-8 Honcho, Kawaguchi, Saitama, 332-0012, Japan;

Graduate School of Natural Science and Technology, Kanazawa University, Kakuma-machi, Kanazawa, 920-1192, Japan;

Graduate School of Natural Science and Technology, Kanazawa University, Kakuma-machi, Kanazawa, 920-1192, Japan;

Graduate School of Natural Science and Technology, Kanazawa University, Kakuma-machi, Kanazawa, 920-1192, Japan;

Graduate School of Natural Science and Technology, Kanazawa University, Kakuma-machi, Kanazawa, 920-1192, Japan;

Graduate School of Natural Science and Technology, Kanazawa University, Kakuma-machi, Kanazawa, 920-1192, Japan;

Graduate School of Natural Science and Technology, Kanazawa University, Kakuma-machi, Kanazawa, 920-1192, Japan;

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专利

1. Conversion from Pillar[5]arene to Pillar[6?15]arenes by Ring Expansion and Encapsulation of C_(60) by Pillar[n]arenes with Nanosize Cavities [J] . Tomoki Ogoshi, Naosuke Ueshima, Fumiyasu Sakakibara, Organic letters . 2014,第11期

机译：通过扩环从柱[5]芳烃转化为柱[6？15]芳烃，并用具有纳米腔的柱[n]芳烃将C_（60）包封
2. Conversion from Pillar[5]arene to Pillar[6?15]arenes by Ring Expansion and Encapsulation of C_(60) by Pillar[n]arenes with Nanosize Cavities [J] . Tomoki Ogoshi, Naosuke Ueshima, Fumiyasu Sakakibara, Organic letters . 2014,第11期

机译：通过扩环从柱[5]芳烃转化为柱[6？15]芳烃，并用具有纳米腔的柱[n]芳烃将C_（60）包封
3. Supramolecular polymers with alternating pillar[5]arene and pillar[6]arene units from a highly selective multiple host-guest complexation system and monofunctionalized pillar[6]arene [J] . Tomoki Ogoshi, Hitoshi Kayama, Daiki Yamafuji Chemical science . 2012,第11期

机译：具有高选择性多主体-客体络合系统和单官能化支柱[6]芳烃的交替支柱[5]芳烃和支柱[6]芳烃单元的超分子聚合物
4. Construction of Expanded Nanotubes via SupramolecularAssembly of Pillar5arenes [C] . Shixin Fa, Yoko Sakata, Shigehisa Akine 日本化学会春季年会 . 2020

机译：通过SupramalularAssembly的柱子构建膨胀纳米管5 arenes
5. Part I. Layered double hydroxides (LDHs): Organic anion exchange reactions, synthesis of microporous pillared derivatives and surface chemistry of metal carbonyl clusters. Part II. On the nature of titania pillared layered silicate clays. [D] . Dimotakis, Emmanuel Dimitrios. 1991

机译：第一部分：层状双氢氧化物（LDHs）：有机阴离子交换反应，微孔柱状衍生物的合成和羰基金属簇的表面化学。第二部分在二氧化钛的性质上有柱状层状硅酸盐粘土。
6. Synthesis of diamido-bridged bis-pillar5arenes and tris-pillar5arenes for construction of unique 1rotaxanes and bis-1rotaxanes [O] . Ying Han, Li-Ming Xu, Cui-Yun Nie, 2018

机译：二酰胺桥联的双立柱5芳烃和三立柱5芳烃的合成用于构建独特的1轮烷和双1轮烷
7. per-Alkoxy-pillar5arenes as Electron Donors: Electrochemical Properties of Dimethoxy-Pillar5arene and Its Corresponding Rotaxane [O] . Nicholas Pearce, E. Stephen Davies, Neil R. Champness 2020

机译：每烷氧基柱5作为电子供体：二甲氧基柱5芳烃的电化学性能及其相应的旋转烷烃

The template effect of solvents on high yield synthesis, co-cyclization of pillar[6]arenes and interconversion between pillar [5]- and pillar[6]arenes

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