Adding a third dimension to operando spectroscopy: a combined UV-Vis, Raman and XAFS setup to study heterogeneous catalysts under working conditions

Beale AM; van der Eerden AMJ; Kervinen K; Newton MA; Weckhuysen BM

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Adding a third dimension to operando spectroscopy: a combined UV-Vis, Raman and XAFS setup to study heterogeneous catalysts under working conditions

机译：在操作光谱学上增加了三维：组合的UV-Vis，Raman和XAFS设置可研究工作条件下的多相催化剂

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摘要

The potential of combined operando UV-Vis/Raman/XAFS has been explored by studying the active site and deactivation mechanism of silica- and alumina-supported molybdenum oxide catalysts under propane dehydrogenation conditions.

机译：通过研究丙烷和脱氢条件下二氧化硅和氧化铝负载的氧化钼催化剂的活性位点和失活机理，探索了组合操作UV-Vis / Raman / XAFS的潜力。

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来源
《Chemical Communications》 |2005年第24期|p. 3015-3017|共3页
作者
Beale AM; van der Eerden AMJ; Kervinen K; Newton MA; Weckhuysen BM;
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作者单位

Univ Utrecht, Debye Inst, Dept Inorgan Chem & Catalysis, NL-3508 TC Utrecht, Netherlands;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
METAL-OXIDE CATALYSTS; SUPPORTED MOLYBDENUM OXIDE; IN-SITU; DEHYDROGENATION;

机译：金属氧化物催化剂;负载型钼氧化物;原位;加氢;

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1. Real-Time Observation of the Defect Dynamics in Working Au/CeO2 Catalysts by Combined Operando Raman/UV-Vis Spectroscopy [J] . Schilling Christian, Hess Christian The journal of physical chemistry, C. Nanomaterials and interfaces . 2018,第5期

机译：组合式Raman / UV-Vis光谱法实时观察Au / CeO2催化剂的缺陷动态
2. Observing Heterogeneous Catalysts While They Are Working Using Operando Raman Spectroscopy [J] . M. Olga Guerrero-Perez, M.A. Banares Spectroscopy . 2012,第10期

机译：使用Operando拉曼光谱法观察异构催化剂的工作情况
3. A combined in situ time-resolved UV-Vis, Raman and high-energy resolution X-ray absorption spectroscopy study on the deactivation behavior of Pt and PtSn propane dehydrogenation catalysts under industrial reaction conditions [J] . Iglesias-Juez A., Beale A.M., Maaijen K., Journal of Catalysis . 2010,第2期

机译：原位时间分辨UV-Vis，拉曼光谱和高能分辨率X射线吸收光谱法研究工业反应条件下Pt和PtSn丙烷脱氢催化剂的失活行为
4. Development of operando PTRF-XAFS Technique for 3D StructureDetermination of Active Metal Species on a Model CatalystSurface under Working Conditions [C] . Bang Lu, Satoru Takakusagi, Daiki Kido 日本化学会春季年会 . 2020

机译：工作条件下模型催化剂曲面上活性金属物种3D结构的Outmando PTRF-XAFS技术的研制
5. Preparation of Silver Catalysts by Atomic Layer Deposition and Studies of Atomic Layer Deposition Reactions Using Operando Surface-Enhanced Raman Spectroscopy. [D] . Masango, Sicelo Simon. 2015

机译：通过原子层沉积制备银催化剂以及使用Operando表面增强拉曼光谱研究原子层沉积反应。
6. Combined Operando X‐ray Diffraction/Raman Spectroscopy of Catalytic Solids in the Laboratory: The Co/TiO2 Fischer–Tropsch Synthesis Catalyst Showcase [O] . Korneel H. Cats, Prof. Dr. Bert M. Weckhuysen -1

机译：实验室中催化固体的Operando X射线衍射/拉曼光谱相结合：Co / TiO2费-托合成催化剂的展示
7. A combined diffuse reflectance infrared Fourier transform spectroscopy–mass spectroscopy–gas chromatography for the operando study of the heterogeneously catalyzed CO2 hydrogenation over transition metal-based catalysts [O] . Kun Zhao, Jie Zhang, Wen Luo, 2020

机译：一种组合的漫反射红外傅里叶变换光谱 - 质谱 - 用于操作同源的转化型CO2氢化过渡金属基催化剂的研究

Adding a third dimension to operando spectroscopy: a combined UV-Vis, Raman and XAFS setup to study heterogeneous catalysts under working conditions

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