A convenient new procedure for converting primary amides into nitriles

Chun-Wei Kuo; Jia-Liang Zhu; Jen-Dar Wu; Cheng-Ming Chu; Ching-Fa Yao; Kak-Shan Shia

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A convenient new procedure for converting primary amides into nitriles

机译：将伯酰胺转化为腈的便捷新方法

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摘要

An operationally simple and high-yielding procedure has been developed for the conversion of primary amides to the corresponding nitriles, using ethyl dichlorophosphate/DBU as the mild dehydrating agent.

机译：使用二氯磷酸乙酯/ DBU作为温和的脱水剂，已开发出一种操作简单且高产的方法，可将伯酰胺转化为相应的腈。

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来源
《Chemical Communications》 |2007年第3期|301-303|共3页
作者
Chun-Wei Kuo; Jia-Liang Zhu; Jen-Dar Wu; Cheng-Ming Chu; Ching-Fa Yao; Kak-Shan Shia;
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作者单位

Division of Biotechnology and Pharmaceutical Research, National Health Research Institutes, Miaoli County, 350, Taiwan, R. O. C.;

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正文语种 eng
中图分类化学;
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入库时间 2022-08-17 13:28:10

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专利

1. A convenient new procedure for converting primary amides into nitriles [J] . Kuo CW, Zhu JL, Wu JD, Chemical Communications . 2007,第3期

机译：将伯酰胺转化为腈的便捷新方法
2. Rapid Method of Converting Primary Amides to Nitriles and Nitriles to Primary Amides by ZnCl_2 using Microwaves under Different Reaction Conditions [J] . Krishnappa Manjula, Mohamed Afzal Pasha Synthetic Communications . 2007,第7a9期

机译：微波在不同反应条件下快速转化伯酰胺为腈和腈由ZnCl_2转化为伯酰胺的快速方法
3. Phenyl chloroformate: A convenient reagent for the preparation of nitriles from primary amides [J] . D Subhas Bose, S Varadarajan, G Vanajatha Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2001,第8期

机译：氯甲酸苯基酯：一种方便的试剂，用于从伯酰胺制备腈
4. Transfer Dehydration of Primary Amides Using Electron-Deficient Nitriles [C] . Hiroyuki Okabe, Takahiro Isogawa, Asuka Naraoka 日本化学会春季年会講演予稿集 . 2018

机译：使用电子缺陷腈转移初级酰胺的脱水
5. I. Solvent-free oxidation of primary ARYL alcohols to aldehydes, and, II. Conversion of primary amide to nitrile using silicon tetrachloride as the dehydrating agent. [D] . Pedraza, Fernando. 2006

机译：I.芳族伯醇无溶剂氧化为醛，以及II。使用四氯化硅作为脱水剂将伯酰胺转化为腈。
6. Development and Utilization of a Palladium-CatalyzedDehydration of Primary Amides To Form Nitriles [O] . MohammedH. Al-Huniti, José Rivera-Chávez, Katsuya L. Colón, -1

机译：钯催化的开发与利用伯酰胺脱水形成腈
7. Triflic Anhydride Promoted Synthesis of Primary Amides and their Conversion into Nitriles [O] . Anil Rana, Varun Kumar, Lata Tiwari, 2018

机译：三氟酸酐促进初级酰胺的合成及其转化为腈

A convenient new procedure for converting primary amides into nitriles

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