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Nd_2O_3 DOPED YTTRIA STABILIZED ZIRCONIA CERAMICS FABRICATED BY CONVENTIONAL AND MICROWAVE SINTERING METHODS

机译:常规微波烧结法制备的Nd_2O_3掺杂钇稳定氧化锆陶瓷。

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Cubic 8 mol. % yuria stabilized zirconia (8YSZ) ceramics doped with 9, 12 and 15 wt. % Nd2O3 were sintered in a single mode 2.45 GHz microwave furnace at sintering temperature of 1400 degrees C for 20 min. and by conventional sintering at 1400 degrees C for 5 h. The microwave sintered samples attained higher densities than the conventional processed ones. The Nd2O3 additions have adverse effects on densification of 8YSZ, ceramics. The XRD investigations revealed that, cubic phase of 8YSZ, remained stable and substitution of Zr4+ ions by larger Nd3+ ions causes an increase in the lattice parameters with Nd2O3 additions. Vickers hairiness of 8YSZ decreased with addition of Nd2O3 irrespective of the sintering technique.
机译:立方8摩尔掺杂了9、12和15 wt。%的尤里里亚稳定的氧化锆(8YSZ)陶瓷。在单模2.45GHz微波炉中在1400℃的烧结温度下烧结%Nd 2 O 3 20分钟。并在1400摄氏度下常规烧结5小时。微波烧结样品的密度高于常规加工样品。 Nd2O3的添加对8YSZ陶瓷的致密化有不利影响。 XRD研究表明,立方相8YSZ保持稳定,并且Zr4 +离子被较大的Nd3 +离子取代会导致添加Nd2O3时晶格参数增加。 Nd2O3的加入会降低8YSZ的维氏毛羽,而与烧结技术无关。

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