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Method for increasing β-SiC yield on solid state reaction of coal fly ash and activated carbon powder

机译:提高粉煤灰与活性炭粉固相反应中β-SiC收率的方法

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摘要

A novel process for increasing β-SiC yield on solid state reaction of coal fly ash and micro powder activated carbon powder has been proposed. β-SiC powder was synthesized at temperature 1300°C for 2 h under vacuum condition with 1 l/min argon flow. Cycling synthesis process has been developed for increasing β-SiC yield on solid state reaction of coal fly ash and activated carbon powder. Synthesized products were analyzed by XRD with Cu-Kα radiation, FTIR spectrometer and SEM fitted with EDAX. The results show that the amount of relative β-SiC is increased with the number of cycling synthesis.
机译:提出了一种提高粉煤灰与微粉活性炭粉固相反应中β-SiC收率的新方法。 β-SiC粉末是在真空条件下,氩气流量为1 l / min的条件下于1300℃下合成2 h的。为了提高粉煤灰与活性炭粉末的固相反应,开发了循环合成工艺以提高β-SiC的收率。合成的产物通过XRD与Cu-Kα辐射,FTIR光谱仪和装有EDAX的SEM进行分析。结果表明,相对β-SiC的含量随着循环合成次数的增加而增加。

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