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Effect of Production Route on the Microstructure and Mechanical Properties of Cu–SiCp Composites

机译:生产路线对Cu–SiCp复合材料组织和力学性能的影响

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摘要

In this study, Cu matrix composite materials reinforced with SiC particles (SiCp) at different contents were produced by two different powder metallurgy (PM) processes, being traditional sintering and hot pressing. For the composites to be produced, 5-25% SiCp by weight was added to pure Cu powder at different contents and powder mixtures were prepared. The mixtures prepared in the production with traditional sintering were shaped by 500 MPa pressure, and green compacts were sintered at different temperatures to determine the optimum sintering conditions. The specimen production with the hot pressing process was performed by keeping the prepared powder mixtures at 880 degrees C, under 20 MPa pressure for 5 min using a graphite mold. The density, microstructure and mechanical properties of the composites produced were examined. The microstructure examinations were performed with the scanning electron microscope, energy distribution spectrometer and X-ray analysis. Characterization techniques such as hardness measurements, 3-point bending test and impact test were used for the determination of mechanical properties. Increased SiCp content caused a decrease in relative density values for both samples produced through traditional sintering method and hot-pressed samples. Considerably high relative density values were achieved with the hot pressing process compared to traditional sintering. The microstructure examinations showed that in the composites produced, the SiCp reinforcement phase dispersed homogeneously in the Cu matrix that comprised of relatively small and equiaxed particles. The mechanical tests showed that hardness increased remarkably with the increasing SiCp content while bending strength and impact energy values decreased.
机译:在这项研究中,通过两种不同的粉末冶金(PM)工艺,即传统的烧结和热压,生产了不同含量的SiCp(SiCp)增强的Cu基复合材料。对于要生产的复合材料,将5-25%重量比的SiCp添加到不同含量的纯铜粉末中,并制备粉末混合物。在传统烧结生产中制备的混合物在500 MPa压力下成型,然后在不同温度下烧结生坯,以确定最佳烧结条件。通过使用石墨模具将制得的粉末混合物在20 MPa压力下于880摄氏度下保持5分钟来进行热压工艺的样品生产。检查了所生产的复合材料的密度,微观结构和机械性能。用扫描电子显微镜,能量分布光谱仪和X射线分析进行显微结构检查。诸如硬度测量,三点弯曲测试和冲击测试之类的表征技术用于确定机械性能。 SiCp含量的增加导致通过传统烧结方法生产的样品和热压样品的相对密度值降低。与传统的烧结相比,通过热压工艺获得了相当高的相对密度值。显微组织检查表明,在生产的复合材料中,SiCp增强相均匀分散在由相对较小且等轴的颗粒组成的Cu基体中。力学测试表明,硬度随着SiCp含量的增加而显着增加,而抗弯强度和冲击能值则降低。

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