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Dispersion behavior of TiB_2 particles in AISI D2 tool steel surfaces during pulsed laser dispersing and their influence on material properties

机译:脉冲激光分散过程中TiSI_2在AISI D2工具钢表面的弥散行为及其对材料性能的影响

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摘要

AISI D2 is one of the most applied cold-working tool steel for deep drawing operations, due to the materials good toughness and high wear resistance. However, since the lubricant-free deep drawing as well as the processing of high strength and ultra-high strength steel sheets remaining ongoing trends in the automotive industry, the tool surfaces need to be improved regarding their friction and wear behavior. For this purpose elevated micro textures can be applied. Since protruded micro features are predominantly affected by wear, a structuring process enabling the formation of suitable textures with high wear resistance is needed.In this paper surface texturing at microscale was conducted by laser implantation. This technique allows the fabrication of highly wear resistant, separated and elevated features (implants) on steel surfaces via a discontinuous dispersing of ceramic particles by pulsed laser radiation. The aim of this study was to investigate the techniques potential for the creation of wear resistant elevated micro features on AISI D2 tool steel surfaces by the application of TiB2 particles. The laser parameters (pulse power and length) were varied and a comparative material analysis on AISI D2 laser remelted spots and TiB2 localized dispersed zones was examined. High-speed camera recordings allowed the description of the particle insertion mechanism from pre-coatings during laser processing. Mechanical properties were analyzed by (micro-) hardness measurements at top and cross sections. The microstructure was investigated by optical microscopy, scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX) and X-ray diffraction (XRD). The implants geometrical properties (diameter, height, depth) were investigated by white light interferometry and optical microscopy. The experiments reveal that a pulsed laser remelting of AISI D2 leads to a significant hardness drop due to high retained austenite (gamma(R)) contents. Contrary, a localized dispersing of TiB2 particles leads to defect free dome- or ring-shaped elevated features with hardness values up to 1800 HV1. The high hardness values result from the dispersed TiB2 particles and an in-situ precipitation of new hard particle phases, which lead to a reduction of the gamma(R) content within the matrix.
机译:AISI D2是用于深冲操作的最常用的冷作工具钢之一,因为该材料具有良好的韧性和高耐磨性。但是,由于无润滑剂的深冲以及高强度和超高强度钢板的加工仍是汽车工业的发展趋势,因此需要改善工具表面的摩擦和磨损性能。为了这个目的,可以应用提高的微纹理。由于突出的微观特征主要受磨损影响,因此需要一种能够形成具有高耐磨性的合适纹理的结构化过程。在本文中,通过激光注入对纸张进行微观表面纹理化。通过脉冲激光辐射对陶瓷颗粒的不连续分散,该技术允许在钢表面上制造高度耐磨,分离且凸起的特征​​(植入物)。这项研究的目的是研究通过使用TiB2颗粒在AISI D2工具钢表面上创建耐磨的高微特征的技术潜力。改变激光参数(脉冲功率和长度),并检查AISI D2激光重熔点和TiB2局部分散区的对比材料分析。高速相机记录允许从激光加工过程中的预涂层描述颗粒插入机制。通过在顶部和横截面的(微)硬度测量来分析机械性能。通过光学显微镜,扫描电子显微镜(SEM),能量色散X射线光谱法(EDX)和X射线衍射(XRD)研究了显微结构。通过白光干涉法和光学显微镜研究了植入物的几何特性(直径,高度,深度)。实验表明,由于高残留奥氏体(gamma)含量,脉冲AISI D2激光重熔会导致硬度显着下降。相反,TiB2颗粒的局部分散会导致无缺陷的圆顶或环形凸起特征,硬度值高达1800 HV1。高硬度值归因于分散的TiB2颗粒和新的硬颗粒相的原位沉淀,这导致了基体中的减少。

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