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Surface-modified antibacterial TiO2/Ag+ nanoparticles: Preparation and properties

机译:表面改性的TiO2 / Ag +抗菌纳米颗粒:制备与性能

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Studies were performed on surface modification of antibacterial TiO2/Ag+ nanoparticles by grafting gamma-aminopropyltriethoxysilane (APS). The interfacial structure of the modified particles was characterized by Fourier-transform infrared spectroscopy, X-ray photoelectron spectroscopy, transmission electron microscopy and thermogravimetric analysis. The thickness of the surface layer was determined by using Auger electron spectroscopy (AES). The results show that APS is chemically bonded to the surface of antibacterial TiO2/Ag+ nanoparticles. Furthermore, the modified particles were mixed in PVC to prepare composites whose antibacterial property was investigated. The results suggest that surface modification has no negative effect on antibacterial activity of TiO2/Ag+ nanoparticles and PVC-TiO2/Ag+ composites exhibits good antibacterial property. (c) 2005 Elsevier B.V. All rights reserved.
机译:通过接枝γ-氨基丙基三乙氧基硅烷(APS)对抗菌TiO2 / Ag +纳米颗粒进行了表面改性研究。通过傅里叶变换红外光谱,X射线光电子能谱,透射电子显微镜和热重分析对改性颗粒的界面结构进行了表征。通过使用俄歇电子能谱法(AES)确定表面层的厚度。结果表明,APS化学键合到抗菌TiO2 / Ag +纳米颗粒的表面。此外,将改性颗粒混合在PVC中以制备其抗菌性能被研究的复合材料。结果表明,表面改性对TiO2 / Ag +纳米颗粒的抗菌活性无不利影响,PVC-TiO2 / Ag +复合材料具有良好的抗菌性能。 (c)2005 Elsevier B.V.保留所有权利。

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