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Surface Characterisation And Electrochemical Behaviour Of Porous Titanium Dioxide Coated 316l Stainless Steel For Orthopaedic Applications

机译:骨科应用多孔二氧化钛涂层316l不锈钢的表面表征和电化学行为

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Porous titanium dioxide was coated on surgical grade 316L stainless steel (SS) and its role on the corrosion protection and enhanced biocompatibility of the materials was studied. X-ray diffraction analysis (XRD), atomic force microscopy (AFM), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and energy dispersive X-ray analysis (EDAX) were carried out to characterise the surface morphology and also to understand the structure of the as synthesised coating on the substrates. The corrosion behaviour of titanium dioxide coated samples in simulated body fluid was evaluated using polarisation and impedance spectroscopy studies. The results reveal that the titanium dioxide coated 316L SS exhibit a higher corrosion resistance than the uncoated 316L SS. The titanium dioxide coated surface is porous, uniform and also it acts as a barrier layer to metallic substrate and the porous titanium dioxide coating induces the formation of hydroxyapatite layer on the metal surface.
机译:多孔二氧化钛被涂覆在外科级316L不锈钢(SS)上,并研究了其在防腐和增强材料生物相容性方面的作用。进行了X射线衍射分析(XRD),原子力显微镜(AFM),傅立叶变换红外(FTIR)光谱,扫描电子显微镜(SEM)和能量色散X射线分析(EDAX),以表征表面形态,并且了解基材上合成涂层的结构。使用极化和阻抗谱研究评估了二氧化钛涂层样品在模拟体液中的腐蚀行为。结果表明,二氧化钛涂覆的316L SS的耐蚀性比未涂覆的316L SS高。二氧化钛涂覆的表面是多孔的,均匀的,并且还充当金属基材的阻挡层,并且多孔的二氧化钛涂层诱导在金属表面上形成羟基磷灰石层。

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