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Development of Epoxy Grout Containing Fine Waste from Production of Mineral Wool Board Insulation

机译:矿棉板保温生产含细废物环氧灌浆的研究

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摘要

Within this work, it was experimentally verified that the waste from mineral wool board insulation production (WIRG) with high portion of glass recyclate (> 80%) and no organic material seems like ideal filler for polymer grouting materials. The main objective was to develop a progressive grout on epoxy basis with as high content of this secondary raw material as possible, while achieving physical and mechanical properties as e.g. very fast strength increase and high thermal resistance. With regard to the consistency of epoxy grout in the fresh state, three different filling were tested, namely 60%, 65% and 70%. The grout with lower filling is too fluid, and it is also disadvantageous from an economic point of view because a large amount of epoxy resin is used. On the other hand, at higher filing, it is not possible to mix the filler into epoxy resin properly. Setting of an optimal filler content in the mixture was performed mostly on the basis of the results of compressive and three-point flexural strength test. It was found out that the optimal amount of the filler is 65%. In case of the best formulation with optimal filler content (65% WIRG), the thermal resistance was monitored by determination of the glass transition temperature (T_g) by the dynamic mechanical analysis (DMA) method. Furthermore, the optical microscope with high resolution was used to monitor filler distribution and homogeneity of the hardened developed epoxy grout.
机译:在这项工作中,通过实验验证了矿棉板绝热生产(WIRG)产生的废料中含有大量的玻璃回收物(> 80%),并且没有有机材料似乎是聚合物灌浆材料的理想填料。主要目的是开发一种基于环氧树脂的渐进灌浆,该灌浆应尽可能多地使用这种次级原料,同时获得物理和机械性能,例如:非常快的强度增加和高耐热性。关于新鲜状态下的环氧树脂灌浆的稠度,测试了三种不同的填充物,即60%,65%和70%。具有较低填充量的灌浆太易流动,并且从经济的角度来看也是不利的,因为使用了大量的环氧树脂。另一方面,在较高的填充量下,不可能将填料适当地混合到环氧树脂中。混合物中最佳填料含量的设定主要基于抗压和三点弯曲强度试验的结果。发现填料的最佳量为65%。对于具有最佳填料含量(65%WIRG)的最佳配方,通过动态力学分析(DMA)方法确定玻璃化转变温度(T_g)来监测热阻。此外,高分辨率的光学显微镜用于监测填料分布和硬化显影环氧灌浆的均匀性。

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