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首页> 外文期刊>Analytical and Bioanalytical Chemistry >Study on the impregnation of archaeological waterlogged wood with consolidation treatments using synchrotron radiation microtomography
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Study on the impregnation of archaeological waterlogged wood with consolidation treatments using synchrotron radiation microtomography

机译:同步辐射显微照相法固结处理浸渍考古木材的研究

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摘要

In favourable conditions of low temperature and low oxygen concentration, archaeological waterlogged wooden artefacts, such as shipwrecks, can survive with a good state of preservation. Nevertheless, anaerobic bacteria can considerably degrade waterlogged wooden objects with a significant loss in polysaccharidic components. Due to these decay processes, wood porosity and water content increase under ageing. In such conditions, the conservation treatments of archaeological wooden artefacts often involve the replacement of water with substances which fill the cavities and help to prevent collapse and stress during drying. The treatments are very often expensive and technically difficult, and their effectiveness very much depends on the chemical and physical characteristics of the substances used for impregnation. Also important are the degree of cavity-filling, penetration depth and distribution in the structure of the wood. In this study, the distribution in wood cavities of some mixtures based on polyethylene glycols and colophony, used for the conservation of waterlogged archaeological wood, was investigated using synchrotron radiation X-ray computed microtomography (SR-μCT). This non-destructive imaging technique was useful for the study of the degraded waterlogged wood and enabled us to visualise the morphology of the wood and the distribution of the materials used in the wood treatments. The study has shown how deposition is strictly related to the dimension of the wooden cavities. The work is currently proceeding with the comparison of synchrotron observations with the data of the solutions viscosity and with those of the properties imparted to the wood by the treatments.
机译:在低温和低氧浓度的有利条件下,沉船等考古渍木制品可以幸存下来并保持良好的保存状态。然而,厌氧细菌可以使浸水的木质物品大大降解,多糖成分的损失也很大。由于这些衰变过程,木材的孔隙度和含水量会随着老化而增加。在这种情况下,考古木制品的保存处理通常包括用填充空腔的物质代替水,并帮助防止干燥过程中的塌陷和应力。这些处理通常很昂贵并且在技术上很困难,其有效性在很大程度上取决于用于浸渍的物质的化学和物理特性。同样重要的是木材结构中空腔的填充程度,穿透深度和分布。在这项研究中,使用同步辐射X射线计算机显微断层照相术(SR-μCT)研究了用于保存浸水考古木材的某些基于聚乙二醇和树脂的混合物在木腔中的分布。这种无损成像技术可用于研究退化的浸水木材,并使我们能够可视化木材的形态和木材处理中所用材料的分布。研究表明,沉积是如何与木腔的尺寸严格相关的。目前正在进行的工作是将同步加速器的观察结果与溶液粘度的数据以及经处理赋予木材的性能进行比较。

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