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Heavy metal detection in mulberry leaves: Laser-induced breakdown spectroscopy data

机译:桑叶中的重金属检测:激光诱导的击穿光谱数据

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摘要

Five copper or chromium stress levels were carried out on mulberry leaf, and 20 samples were collected for each metal stress level. A total of 100 samples (copper or chromium) were processed into uniform pressed pellet. The mulberry leaf pellet was placed on a sample platform of laser-induced breakdown spectroscopy (LIBS) system. A laser was used to ablate the sample pellet and generate the emission lines, the intensity and delay time of laser ablation were 80 mJ and 4 μs respectively. To reduce the acquisition errors, 16 different positions of each sample were ablated for 5 accumulation. Then, 80 spectra were collected per sample and the average of them was considered as the sample spectrum for subsequent analysis. Finally, a total of 200 spectra of copper and chromium in mulberry leaves with a wavelength range of 219–877 nm were obtained for calibration analysis [1].
机译:在桑树叶上进行五种铜或铬胁迫水平,针对每个金属应激水平收集20个样品。将总共​​100个样品(铜或铬)加工成均匀的压制颗粒。将桑叶颗粒置于激光诱导的击穿光谱(LIBS)系统的样本平台上。使用激光烧蚀样品颗粒并产生发射线,激光烧蚀的强度和延迟时间分别为80MJ和4μs。为了减少采集​​误差,将每个样品的16个不同的位置烧蚀5个累积。然后,每个样品收集80个光谱,并且它们的平均值被认为是随后分析的样品光谱。最后,在校准分析中获得了总共200颗铜和铬的铜和铬,具有219-877nm的波长范围[1]。

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