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Cellulose Nanofibers Isolated from the Cuscuta Reflexa Plant as a Green Reinforcement of Natural Rubber

机译:从弯角Re植物分离的纤维素纳米纤维作为天然橡胶的绿色增强

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摘要

In the present work, we used the steam explosion method for the isolation of cellulose nanofiber (CNF) from , a parasitic plant commonly seen in Kerala and we evaluated its reinforcing efficiency in natural rubber (NR). Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), and Thermogravimetric analysis (TGA) techniques indicated that type I cellulose nanofibers, with diameter: 10–30 nm and a 67% crystallinity index were obtained by the proposed method. The results showed that application of CNF in NR based nanocomposites resulted in significant improvement of their processing and performance properties. It was observed that the tensile strength and tear strength of NR/CNF nanocomposites are found to be a maximum at 2 phr CNF loading, which corresponds with the studies of equilibrium swelling behavior. Dynamic mechanical analysis, thermogravimetric analysis, and morphological studies of tensile fractured samples also confirm that CNF isolated from plant can be considered as a promising green reinforcement for rubbers.
机译:在本工作中,我们使用蒸汽爆炸法从喀拉拉邦常见的寄生植物中分离出纤维素纳米纤维(CNF),并评估了其在天然橡胶(NR)中的增强效率。傅立叶变换红外光谱(FTIR),X射线衍射(XRD),扫描电子显微镜(SEM),透射电子显微镜(TEM)和热重分析(TGA)技术表明,直径为10–30的I型纤维素纳米纤维通过所提出的方法获得了100nm和67%的结晶度指数。结果表明,CNF在NR基纳米复合材料中的应用显着改善了其加工性能和性能。观察到,在2phr CNF载荷下,NR / CNF纳米复合材料的拉伸强度和撕裂强度最大,这与平衡溶胀行为的研究相对应。拉伸断裂样品的动态力学分析,热重分析和形态研究也证实,从植物中分离出的CNF可以被认为是橡胶的有希望的绿色增强剂。

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