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Nano-Indentation Response of Ultrahigh Molecular Weight Polyethylene (UHMWPE): A Detailed Analysis

机译:超高分子量聚乙烯(UHMWPE)的纳米压痕响应:详细分析

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摘要

Nano-indentation, a depth sensing technique, is a useful and exciting tool to investigate the surface mechanical properties of a wide range of materials, particularly polymers. Knowledge of the influence of experimental conditions employed during nano-indentation on the resultant nano-mechanical response is very important for the successful design of engineering components with appropriate surface properties. In this work, nano-indentation experiments were carried out by selecting various values of frequency, amplitude, contact depth, strain rate, holding time, and peak load. The results showed a significant effect of amplitude, frequency, and strain rate on the hardness and modulus of the considered polymer, ultrahigh molecular weight polyethylene (UHMWPE). Load-displacement curves showed a shift towards the lower indentation depths along with an increase in peak load by increasing the indentation amplitude or strain rate. The results also revealed the strong dependence of hardness and modulus on the holding time. The experimental data of creep depth as a function of holding time was successfully fitted with a logarithmic creep model (R ≥ 0.98). In order to remove the creeping effect and the nose problem, recommended holding times were proposed for the investigated polymer as a function of different applied loads.
机译:纳米压痕技术是一种深度感测技术,是研究各种材料(特别是聚合物)的表面机械性能的有用且令人兴奋的工具。知道在纳米压痕过程中采用的实验条件对所得纳米机械响应的影响,对于成功设计具有适当表面特性的工程组件非常重要。在这项工作中,通过选择各种频率,振幅,接触深度,应变率,保持时间和峰值负载的值进行了纳米压痕实验。结果表明,振幅,频率和应变率对所考虑的聚合物,超高分子量聚乙烯(UHMWPE)的硬度和模量有显着影响。载荷-位移曲线表明,随着压痕振幅或应变速率的增加,压痕深度逐渐减小,峰值载荷增加。结果还表明硬度和模量对保持时间的强烈依赖性。将蠕变深度作为保持时间的函数的实验数据成功地拟合了对数蠕变模型(R≥0.98)。为了消除蠕变效应和鼻部问题,建议将所研究的聚合物的建议保持时间作为不同施加载荷的函数。

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