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Modification of the Interface Nanostructure and Magnetic Properties in Nd-Fe-B Thin Films

机译:Nd-Fe-B薄膜中界面纳米​​结构和磁性能的改性

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摘要

The effects of Nd2Fe14B grain size and Nd coating on the coercivity in sputter-deposited Nd-Fe-B/Nd thin films have been investigated in order to gain an insight into the coercivity mechanism of Nd-Fe-B magnets. Highly textured Nd2Fe14B particles were grown successfully on the MgO(100) single-crystal substrate with the Mo underlayer. As the Nd-Fe-B layer thickness tNFB was decreased from 70 to 5 nm, the coercivity Hc increased gradually from 6.5 to 16 kOe. By depositing the Nd overlayer onto these films and post-annealing at 500 °C, the Hc value further increased from 17.5 kOe (tNFB=70 nm) to 26.2 kOe (tNFB=5 nm). The amount of Hc increase by the combination of the Nd coating and post-annealing was about 10 kOe irrespective of the tNFB value. These results therefore suggest an independence of size and interface effects on the coercivity of Nd-Fe-B magnets.
机译:为了了解Nd-Fe-B磁体的矫顽力机理,研究了Nd2Fe14B晶粒尺寸和Nd涂层对溅射沉积Nd-Fe-B / Nd薄膜矫顽力的影响。高度织构化的Nd2Fe14B粒子在具有Mo底层的MgO(100)单晶衬底上成功生长。随着Nd-Fe-B层厚度tNFB从70 nm减小到5 nm,矫顽力Hc从6.5 kOe逐渐增加。通过将Nd覆盖层沉积到这些薄膜上并在500°C下进行退火,Hc值进一步从17.5 kOe(tNFB = 70 nm)增至26.2 kOe(tNFB = 5 nm)。 Nd涂层和后退火相结合的Hc增加量约为10 kOe,而与tNFB值无关。因此,这些结果表明尺寸和界面效应对Nd-Fe-B磁体的矫顽力具有独立性。

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