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Morphological Structure Rheological Behavior Mechanical Properties and Sound Insulation Performance of Thermoplastic Rubber Composites Reinforced by Different Inorganic Fillers

机译:不同无机填料增强热塑性橡胶复合材料的形态结构流变行为力学性能和隔音性能

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摘要

The application area of a sound insulation material is highly dependent on the technology adopted for its processing. In this study, thermoplastic rubber (TPR, polypropylene/ethylene propylene diene monomer) composites were simply prepared via an extrusion method. Two microscale particles, CaCO3 and hollow glass microspheres (HGW) were chosen to not only enhance the sound insulation but also reinforced the mechanical properties. Meanwhile, the processing capability of composites was confirmed. SEM images showed that the CaCO3 was uniformly dispersed in TPR matrix with ~3 μm scale aggregates, while the HGM was slightly aggregated to ~13 μm scale. The heterogeneous dispersion of micro-scale fillers strongly affected the sound transmission loss (STL) value of composites. The STL values of TPR composites with 40 wt % CaCO3 and 20 wt % HGM composites were about 12 dB and 7 dB higher than that of pure TPR sample, respectively. The improved sound insulation performances of the composites have been attributed to the enhanced reflection and dissipate sound energy in the heterogeneous composite. Moreover, the mechanical properties were also enhanced. The discontinued sound impedance and reinforced stiffness were considered as crucial for the sound insulation.
机译:隔音材料的应用领域在很大程度上取决于其加工所采用的技术。在这项研究中,热塑性橡胶(TPR,聚丙烯/乙烯丙烯二烯单体)复合材料是通过挤出方法简单地制备的。选择了两个微米级的颗粒,CaCO3和空心玻璃微球(HGW),不仅增强了隔音效果,而且增强了机械性能。同时,证实了复合材料的加工能力。 SEM图像显示,CaCO3均匀分散在TPR基质中,聚集体约为〜3μm,而HGM略微聚集至〜13μm。微米级填料的不均匀分散强烈影响复合材料的声传输损耗(STL)值。具有40 wt%CaCO3和20 wt%HGM复合材料的TPR复合材料的STL值分别比纯TPR样品高约12 dB和7 dB。复合材料的改进的隔音性能归因于非均质复合材料中增强的反射和消散声能。而且,机械性能也得到提高。不连续的声阻抗和增强的刚度被认为是隔音的关键。

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