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Mechanical Vibration Measurement of Solidly Mounted Resonator in Fluid by Atomic Force Microscopy

机译:固体力共振器在流体中的机械振动原子力显微镜测量

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摘要

The very small vibration of a solidly-mounted resonator (SMR) in fluid may trigger a relatively large motion of the covering fluid, which was implied by our protein-related experimental results. Therefore, a series of experimental methods for characterizing the mechanical longitudinal vibration of the SMR and the corresponding out-of-plane dynamic response of the fluid above the SMR surface is described in this paper. A SMR device with theoretical resonance frequency of 2.5 GHz was driven by an amplitude-modulated (AM) signal, in which the amplitude is modulated by a signal of the second resonance frequency of the atomic force microscope (AFM) cantilever. A lock-in amplifier is used to demodulate the vibration response of the AFM cantilever, which is proportional to the amplitude of the sample vibration in contact mode and tapping mode. The amplitude-frequency curve of the SMR surface is obtained in contact mode with a relatively stronger interaction force between the AFM tip and the SMR surface. The amplitude-frequency curve of the motion of the liquid above the SMR device and the peak amplitude of the fluid at different distances above the SMR surface are measured in tapping mode with a relatively weak interaction force between the AFM tip and the fluid sample.
机译:固体安装的谐振器(SMR)在流体中的很小振动可能会触发覆盖流体的相对较大运动,这与我们与蛋白质相关的实验结果暗示了这一点。因此,本文描述了一系列表征SMR的机械纵向振动以及SMR表面上方流体的平面外动态响应的实验方法。理论谐振频率为2.5 GHz的SMR器件由调幅(AM)信号驱动,其中幅度由原子力显微镜(AFM)悬臂的第二谐振频率的信号调制。锁定放大器用于解调AFM悬臂的振动响应,该响应与接触模式和敲击模式下样品振动的幅度成比例。在AFM尖端和SMR表面之间具有相对较强的相互作用力的情况下,以接触模式获得SMR表面的振幅-频率曲线。在攻丝模式下,在AFM尖端与流体样品之间的相互作用力相对较弱的情况下,测量了SMR装置上方的液体运动的幅度-频率曲线以及SMR表面上方不同距离处的流体的峰值幅度。

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