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Transient Liquid Phase Bonding of Ti-6Al-4V and Mg-AZ31 Alloys Using Zn Coatings

机译:使用锌涂层的Ti-6Al-4V和Mg-AZ31合金的瞬时液相键合

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摘要

Ti-6Al-4V and Mg-AZ31 were bonded together using the Transient Liquid Phase Bonding Process (TLP) after coating both surfaces with zinc. The zinc coatings were applied using the screen printing process of zinc paste. Successful bonds were obtained in a vacuum furnace at 500 °C and under a uniaxial pressure of 1 MPa using high frequency induction heat sintering furnace (HFIHS). Various bonding times were selected and all gave solid joints. The bonds were successfully achieved at 5, 10, 15, 20, 25, and 30 min. The energy dispersive spectroscopy (EDS) line scan confirmed the diffusion of Zn in both sides but with more diffusion in the Mg side. Diffusion of Mg into the joint region was detected with significant amounts at bonds made for 20 min and above, which indicate that the isothermal solidification was achieved. In addition, Ti and Al from the base alloys were diffused into the joint region. Based on microstructural analysis, the joint mechanism was attributed to the formation of solidified mixture of Mg and Zn at the joint region with a presence of diffused Ti and Al. This conclusion was also supported by structural analysis of the fractured surfaces as well as the analysis across the joint region. The fractured surfaces were analyzed and it was concluded that the fractures occurred within the joint region where ductile fractures were observed. The strength of the joint was evaluated by shear test and found that the maximum shear strength achieved was 30.5 MPa for the bond made at 20 min.
机译:用锌涂覆两个表面后,使用瞬态液相键合工艺(TLP)将Ti-6Al-4V和Mg-AZ31键合在一起。锌涂层是使用锌浆的丝网印刷工艺施加的。使用高频感应热烧结炉(HFIHS)在500°C的真空炉中和1 MPa的单轴压力下获得成功的粘结。选择各种粘结时间,所有粘结时间均牢固。在5、10、15、20、25和30分钟时成功实现了键合。能量色散谱(EDS)线扫描证实了Zn在两侧都有扩散,但在Mg侧有更多的扩散。在20分钟及20分钟以上的粘结时,检测到大量的Mg扩散进入接头区域,这表明已实现了等温固化。另外,来自基础合金的Ti和Al扩散到接合区域中。基于微观结构分析,这种连接机理归因于在存在扩散的Ti和Al的连接区域形成了Mg和Zn的凝固混合物。断裂表面的结构分析以及整个接缝区域的分析也支持了这一结论。分析了断裂的表面,得出的结论是,断裂发生在观察到延性断裂的接头区域内。通过剪切试验评估了接头的强度,发现在20分钟时完成的粘结所达到的最大剪切强度为30.5 MPa。

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