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Microstructural Evolution and Refinement Mechanism of a Beta–Gamma TiAl-Based Alloy during Multidirectional Isothermal Forging

机译:β-γTiAl基合金在多向等温锻造过程中的组织演变及细化机理

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摘要

Multidirectional isothermal forging (MDIF) was used on a Ti-44Al-4Nb-1.5Cr-0.5Mo-0.2B (at. %) alloy to obtain a crack-free pancake. The microstructural evolution, such as dynamic recovery and recrystallization behavior, were investigated using electron backscattered diffraction and transmission electron microscopy methods. The MDIF broke down the initial near-lamellar microstructure and produced a refined and homogeneous duplex microstructure. γ grains were effectively refined from 3.6 μm to 1.6 μm after the second step of isothermal forging. The ultimate tensile strength at ambient temperature and the elongation at 800 °C increased significantly after isothermal forging. β/B2→α2 transition occurred during intermediate annealing, and α2 + γ→β/B2 transition occurred during the second step of isothermal forging. The refinement mechanism of the first-step isothermal forging process involved the conversion of the lamellar structure and discontinuous dynamic recrystallization (DDRX) of γ grains in the original mixture-phase region. The lamellar conversion included continuous dynamic recrystallization and DDRX of the γ laths and bugling of the γ phase. DDRX behavior of γ grains dominated the refinement mechanism of the second step of isothermal forging.
机译:在Ti-44Al-4Nb-1.5Cr-0.5Mo-0.2B(at。%)合金上使用多向等温锻造(MDIF),以获得无裂纹的煎饼。使用电子背散射衍射和透射电子显微镜方法研究了微观结构的演变,例如动态恢复和再结晶行为。 MDIF破坏了最初的近层微结构,并产生了细化且均匀的双相微结构。经过第二步等温锻造后,γ晶粒有效地从3.6μm细化到1.6μm。等温锻造后,在室温下的极限抗拉强度和在800°C下的伸长率显着提高。 β/ B2→α2相变在中间退火过程中发生,而α2+γ→β/ B2相变在等温第二步锻造过程中发生。第一步等温锻造工艺的细化机理包括层状结构的转变和原始混合相区域中γ晶粒的不连续动态重结晶(DDRX)。层状转变包括γ板条的连续动态重结晶和DDRX以及γ相的脆化。 γ晶粒的DDRX行为主导了第二步等温锻造的细化机理。

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