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Fabrication of Cu Based Metallic Binder for Diamond Tools by Microwave Pressureless Sintering

机译:微波无压烧结制备金刚石工具用铜基金属粘结剂

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摘要

Microwave pressureless sintering (MPS) method is successfully applied in the fabrication of Cu based metallic matrix for diamond tools. The main purpose of this work is to obtain better mechanical properties when the metal binder of the diamond tools was prepared by the MPS method. The orthogonal experimental method is adopted to design the sintering process parameters. The optimized experimental conditions are suggested as 880 °C of sintering temperature, 375 MPa of cold pressure, and 35 min of withholding time. The contrastive investigation of the MPS and conventional pressureless sintering (CPS) are performed under optimized conditions. The microstructures information are obtained by scanning electron microscopy (SEM), X-ray diffraction (XRD), electron probe microanalysis (EPMA), and the necessary mechanical properties, such as relative density, hardness, and flexural strength are tested. Experimental results show that the MPS method, compared with CPS, can significantly improve the mechanical properties of the metallic matrix. The factors of relative density, hardness, and flexural strength increase 1.25%, 3.86%, and 6.28%, respectively. The possible sintering mechanism of the MPS method is also discussed. This work may provide a reference for the fabrication of metal-based diamond tools by microwave heating method.
机译:微波无压烧结(MPS)方法已成功应用于金刚石工具的铜基金属基体的制造中。这项工作的主要目的是在通过MPS方法制备金刚石工具的金属粘结剂时获得更好的机械性能。采用正交试验法设计了烧结工艺参数。建议的最佳实验条件为:烧结温度为880°C,冷压为375 MPa,保留时间为35分钟。 MPS和常规无压烧结(CPS)的对比研究是在优化条件下进行的。通过扫描电子显微镜(SEM),X射线衍射(XRD),电子探针显微分析(EPMA)获得微观结构信息,并测试必要的机械性能,例如相对密度,硬度和抗弯强度。实验结果表明,与CPS相比,MPS方法可以显着改善金属基体的机械性能。相对密度,硬度和抗弯强度的因素分别增加了1.25%,3.86%和6.28%。还讨论了MPS方法可能的烧结机理。这项工作可为通过微波加热方法制造金属基金刚石工具提供参考。

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