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Microstructure Characterization and Wear-Resistant Properties Evaluation of an Intermetallic Composite in Ni–Mo–Si System

机译:Ni-Mo-Si体系中金属间化合物的显微组织表征和耐磨性能评估

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摘要

Intermetallic compounds have been studied for their potential application as structural wear materials or coatings on engineering steels. In the present work, a newly designed intermetallic composite in a Ni–Mo–Si system was fabricated by arc-melting process with commercially pure metal powders as starting materials. The chemical composition of this intermetallic composite is 45Ni–40Mo–15Si (at %), selected according to the ternary alloy diagram. The microstructure was characterized using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive spectroscopy (EDS), and the wear-resistant properties at room temperature were evaluated under different wear test conditions. Microstructure characterization showed that the composite has a dense and uniform microstructure. XRD results showed that the intermetallic composite is constituted by a binary intermetallic compound NiMo and a ternary Mo2Ni3Si metal silicide phase. Wear test results indicated that the intermetallic composite has an excellent wear-resistance at room-temperature, which is attributed to the high hardness and strong atomic bonding of constituent phases NiMo and Mo2Ni3Si.
机译:已经研究了金属间化合物作为结构耐磨材料或工程钢涂层的潜在应用。在目前的工作中,以商业纯金属粉末为起始原料,通过电弧熔化工艺在Ni-Mo-Si系统中制备了一种新设计的金属间化合物。该金属间化合物的化学成分为45Ni-40Mo-15Si(原子%),根据三元合金图选择。使用光学显微镜(OM),扫描电子显微镜(SEM),X射线衍射(XRD)和能量色散光谱(EDS)对显微组织进行表征,并在不同的磨损测试条件下评估室温下的耐磨性能。 。微观结构表征表明该复合材料具有致密且均匀的微观结构。 XRD结果表明,金属间化合物由二元金属间化合物NiMo和三元Mo2Ni3Si金属硅化物相组成。磨损试验结果表明,金属间复合材料在室温下具有优异的耐磨性,这归因于组成相NiMo和Mo2Ni3Si的高硬度和牢固的原子键合。

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