In order to study high-frequency soft magnetic properties of Finemet amorphous alloy,the microstructural change and nanocrystallization under different heat treatment conditions were investigated by XRD and TEM. The crystallite size of α-Fe was calculated from the XRD pattern using the Scherrer formula,while the high frequency magnetic properties were measured at room temperature by TPS-200SA exchange tester. The results of XRD and TEM indicate that the nanocrystallization occurs at 500 ℃. When the annealing temperature increases to 560 ℃,the amorphous alloy becomes totally nanocrystallized and the crystallites distribute homogeneously,thus an excellent combination of soft magnetic properties is obtained.
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