火花源原子发射光谱法分析铸铝合金的化学成分

摘要

The chemical composition of ZAL cast-aluminum alloy was comprehensively analyzed by spark source atomic emission spectrometry.The working conditions of instrument such as the precombustion time, integration time and cleaning time of electrode were optimized.The appropriate two-spot standardized samples were used to find the calibration method for the simultaneous determination of chemical composition in ZAL cast-aluminum alloy.The proposed method was applied to the determination of Cu, Mn, Zn, Pb, Mg, Sn, Fe, Cr, Ni, Ti and Si in cast-aluminum alloy.The results were in good agreement with the certified values.%用火花源原子发射光谱仪对ZAL铸铝合金的化学成分进行全分析.通过实验确定了予燃时间、积分时间、对电极清理时间等最佳的仪器工作条件,并在最佳工作条件下,选取了适宜的两点标准化试样,给出了适合ZAL铸铝合金中化学成分同时测定的校准方案.所建立的方法应用于铸铝合金中Cu,Mn,Zn,Pb,Mg,Sn,Fe,Cr,Ni,Ti,Si等元素的测定,测得结果与认定值一致.