Micrometer NbCx-C three-dimensional netted fibers were synthesized by the carbothermal method under 0. 1 MPa of N, ambient atmosphere at a relatively low temperature. Raw materials were commercial powders of Nb205(99.95%), reactive carbon(99.99%), NaC1(99.95%) and sucrose(99.94%). The relationship of the fabrication processing with the composition, crystal structure and morphology of fibers was investigated. The formation mechanism was also proposed and discussed.
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