Preparation method of photocatalyst, using TiCl4 and SnCl2 as raw material and photocatalytic activity of nano-scaled core-shell Sn2+-doped titania photocatalyst was studied in this paper. The as-prepared samples were studied by UV-Vis, XRD, XPS, TEM. The particles of Sn2+-doped TiO2 photocatalyst, calcined from 150 to 600 °C for 5 h, possesses narrow particle size distribution and the sample was composed of anatase phase. Its photocatalytic efficiency was investigated by UV irradiation.
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