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Study on Modification of Ultra-Stable Zeolite Prepared by Hydrothermal Method

机译:水热法制备超稳定沸石的改性研究

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摘要

The ultra-stable zeolite DASY-0.0 was prepared by hydrothermal method in commercial scale.Its structure was further modified via the treatment for cleaning of pores(CP).The zeolite samples before and after CP treating were analyzed and characterized by XRF,XRD,NMR,IR,BET and DTA.The results showed that,in comparison with the conventional ultra-stable zeolite DASY-0.0 prepared by the hydrothermal process,the CP-modified zeolite SOY0 exhibited a higher relative crystallinity.a larger surface area and pore volume,a higher thermal stability and contained less amorphous non-framework Al.
机译:通过水热法以商业规模制备超稳定沸石DASY-0.0,并通过清洁毛孔(CP)的处理对其结构进行了进一步修饰.CP处理前后的沸石样品通过XRF,XRD, NMR,IR,BET和DTA分析表明,与水热法制备的常规超稳定沸石DASY-0.0相比,CP改性沸石SOY0具有较高的相对结晶度,较大的表面积和孔体积。 ,具有较高的热稳定性,并含有较少的非晶态非骨架Al。

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