STUDIES ON THE REACTION OF SULFUR,SELENIUM AND TELLURIUM WITH SODIUM HYDROXIDE UNDER PHASE TRANSFER CATALYSIS(Ⅱ).A CONVENIENT METHOD FOR THE SYNTHESIS OF BI(ACYL)DISULFIDES

Jin-Xian WANG(Chin-Hsien WANG) Wenfeng CUI Yulai HU Kai ZHAO Institute of ChemistryDepartment of ChemistryNorthwest Normal UniversityLanzhou730070

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STUDIES ON THE REACTION OF SULFUR,SELENIUM AND TELLURIUM WITH SODIUM HYDROXIDE UNDER PHASE TRANSFER CATALYSIS(Ⅱ).A CONVENIENT METHOD FOR THE SYNTHESIS OF BI(ACYL)DISULFIDES

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A simple and general method for the synthesis of bi(acyl)disulfides isreported.Sulfur is allowed to react with sodium hydroxide to give sodium disulfideat 65℃ under PTC,which can react with acyl halides to afford bi(acyl)disulfides ingood to excellent isolated yields.The effects of solvents and phase transfercatalysts are discussed.

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《中国化学快报：英文版》|1990年第3期|193-196|共4页
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Jin-Xian WANG(Chin-Hsien WANG) Wenfeng CUI Yulai HU Kai ZHAO Institute of ChemistryDepartment of ChemistryNorthwest Normal UniversityLanzhou730070;
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正文语种 chi
中图分类化学;
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react; afford; allowed; hydroxide; Sulfur; benzoyl; sulfur; 云一; Victor; tentative;
入库时间 2022-08-21 01:32:21

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1. SYNTHESIS OF 1-O-ACYL-2,3,4-TRI-O-ACETYL-β-D-XYLO-AND ARABINOPYRANOSES BY PHASE TRANSFER CATALYSIS [J] . Guan Zhong SHUN~* and Liang Ju XUE Chemistry DepartmentXinjiang UniversityUrumqi830046 . 中国化学快报：英文版 . 1992,第3期

STUDIES ON THE REACTION OF SULFUR,SELENIUM AND TELLURIUM WITH SODIUM HYDROXIDE UNDER PHASE TRANSFER CATALYSIS(Ⅱ).A CONVENIENT METHOD FOR THE SYNTHESIS OF BI(ACYL)DISULFIDES

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