IN-SITU REFLECTION MICROSCOPIC FTIR SPECTROELECTROCHEMISTRY AT MICRO-/ULTRAMICROELECTRODE

摘要

An in-situ reflection ultramicroelectrode microscopic FTIR spectroelectrochemicalcell was constructed and demonstrated by using hexacyanoferrate redox couple in aqueoussulphate solution.An excellent microscopic SNIFTIRS reflection spectra had been obtainedwith no difficulty of IR beam focusing.The cell is simple in construction and convenient foruse,And it will have most of all advantages of micro-/ultramicroelectrode.