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Dynamic behavior of zirconia ceramics in uniaxial compression.

机译:氧化锆陶瓷的单轴压缩动力学行为。

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摘要

A novel Split Hopkinson Pressure Bar (SHPB) method called the stress reversal Hopkinson technique developed at UCSD, is successfully used to subject ceramic samples to predetermined compressive stress pulses. The advantage of the technique is that the ceramics are subjected to a single well-defined compressive stress pulse of approximately 60 {dollar}mu{dollar}s duration, and then recovered for further analysis. Unlike the traditional SHPB method, in this technique the compressive pulse is immediately followed by a tensile pulse. After the compressive pulse loads the sample, all other pulses which travel towards the sample are tensile and hence the sample is not reloaded.; Transformation plasticity in Magnesia-Partially Stabilized Zirconia (Mg-PSZ) and Yttria-Tetragonal Zirconia Polycrystal (Y-TZP) is investigated in this study. The samples tested in SHPB show a tri-linear stress-strain behavior. The longitudinal and transverse strains are measured by strain gages mounted on the samples. The lateral surfaces of Mg-PSZ samples show extensive surface rumpling and microcracking parallel to the loading axis after the test. Reloading of these samples to higher stress levels did not reveal additional inelasticity. Cuboid samples which have been loaded initially to attain transformation saturation, are then reloaded in a direction perpendicular to the first loading. The second loading produces additional inelasticity and microcracking (parallel to this loading direction), indicating the formation of transformation texture in each loading under uniaxial compression. Scanning electron microscope (SEM) observations on suitably etched samples reveal evidence of isolated and correlated transformations. Transmission electron microscope (SEM) observations reveal crack deflection around the precipitates and microcracking around transversely twinned precipitates. X-ray diffraction (XRD) on these samples shows significant monoclinic peaks and reduced tetragonal peaks. Ultrasonic measurements on samples subjected to different stress levels indicate decreased modulus due to microcracking. A micromechanical damage model for modulus degradation of a cracked body is developed using the assumption of dilute distribution of cracks, and the results are compared with the ultrasonic measurements. A micromechanical phenomenological model is also developed to predict the transformation strains and uniaxial stress-strain behavior assuming a potency distribution for the particles. The resulting stress-strain curves are in good agreement with the experimentally obtained curves.
机译:UCSD开发的一种称为“应力逆转霍普金森技术”的新颖的“分裂霍普金森压力棒”(SHPB)方法已成功用于对陶瓷样品施加预定的压缩应力脉冲。该技术的优点是使陶瓷经受单个持续时间大约为60μs的明确定义的压缩应力脉冲,然后将其回收用于进一步分析。与传统的SHPB方法不同,在此技术中,压缩脉冲紧随其后是拉伸脉冲。在压缩脉冲加载样品后,所有向样品传播的其他脉冲均处于拉伸状态,因此不会重新加载样品。本研究研究了镁-部分稳定的氧化锆(Mg-PSZ)和氧化钇-四方氧化锆多晶(Y-TZP)的转变可塑性。 SHPB中测试的样品显示出三线性应力-应变行为。纵向和横向应变通过安装在样品上的应变计测量。测试后,Mg-PSZ样品的侧面显示出大的表面起皱和平行于加载轴的微裂纹。将这些样品重新加载到更高的应力水平并没有显示出额外的弹性。最初已加载以达到转换饱和的长方体样本然后在垂直于第一次加载的方向上重新加载。第二次加载会产生额外的非弹性和微裂纹(平行于此加载方向),表明在单轴压缩下的每个加载中均会形成变形纹理。在适当蚀刻的样品上的扫描电子显微镜(SEM)观察结果揭示了分离和相关转化的证据。透射电子显微镜(SEM)的观察结果表明,析出物周围出现裂纹偏转,横向孪晶析出物周围出现微裂纹。这些样品的X射线衍射(XRD)显示出明显的单斜峰和减少的四方峰。对经受不同应力水平的样品进行超声测量表明,由于微裂纹,模量降低。基于裂纹的稀薄分布的假设,建立了裂纹体模量退化的微机械损伤模型,并将结果与​​超声测量结果进行了比较。还建立了微机械现象学模型,以假设颗粒的效能分布来预测转变应变和单轴应力-应变行为。所得的应力-应变曲线与实验获得的曲线非常吻合。

著录项

  • 作者

    Ghatuparthi, Subhash.;

  • 作者单位

    University of California, San Diego.;

  • 授予单位 University of California, San Diego.;
  • 学科 Applied Mechanics.; Engineering Materials Science.
  • 学位 Ph.D.
  • 年度 1991
  • 页码 145 p.
  • 总页数 145
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 应用力学;工程材料学;
  • 关键词

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