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Fabrication of magnesium matrix composites using a spontaneous infiltration technique.

机译:使用自发渗透技术制备镁基复合材料。

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摘要

A new process was developed to fabricate particulate metal matrix composites (MMCs). The process involves two steps: (1) forming a particulate porous compact, and (2) introducing molten magnesium or magnesium alloy (AZ91) into the channel network by a spontaneous infiltration technique.; A uniform distribution of SiC particulates in magnesium matrix was achieved. Microsegregation existed in composites when the particle size of reinforcement was 38 mum and 22 mum, however, when the particle size of reinforcement was 12 mum, the microsegregation was eliminated.; The interfacial reaction between SiC and Mg studied by Scanning Electron Microscopy (SEM), microanalysis, and X-Ray Diffraction (XRD) techniques showed that, Mg reacted with Si or SiO2 to form Mg2Si, Mg 2Si was present at the surface of SiC after precipitation, resulting in improved wettability between Mg and SiC. As a result of this interfacial reaction, the infiltration process became spontaneous. The infiltration process was related to the infiltration temperature, SiC particle size and matrix chemistry. Increasing the infiltration temperature, decreasing the particle size of SiC resulted in more successful infiltration.; Mechanical testing conducted on composites revealed that the hardness and Ultimate Tensile Strength (UTS) of composites increased with the decrease of particle size of SiC and corresponded to an increase of the volume fraction of SiC.
机译:开发了一种新工艺来制造颗粒状金属基复合材料(MMC)。该过程包括两个步骤:(1)形成颗粒状多孔压块,(2)通过自发渗透技术将熔融的镁或镁合金(AZ91)引入通道网络中。 SiC颗粒在镁基体中的分布均匀。当增强体的粒径为38μm和22μm时,复合物中存在微偏析,然而,当增强体的粒径为12μm时,则消除了微偏析。通过扫描电子显微镜(SEM),显微分析和X射线衍射(XRD)技术研究了SiC与Mg之间的界面反应,结果表明,Mg与Si或SiO2反应形成Mg2Si,Mg2Si存在于SiC表面。沉淀,从而改善了Mg与SiC之间的润湿性。这种界面反应的结果是渗透过程是自发的。渗透过程与渗透温度,SiC颗粒尺寸和基质化学有关。提高渗透温度,减小SiC的粒径,可使渗透更加成功。对复合材料进行的机械测试表明,复合材料的硬度和极限拉伸强度(UTS)随着SiC颗粒尺寸的减小而增加,并且与SiC体积分数的增加相对应。

著录项

  • 作者

    Chen, Huiqiang.;

  • 作者单位

    McGill University (Canada).;

  • 授予单位 McGill University (Canada).;
  • 学科 Engineering Materials Science.
  • 学位 M.Eng.
  • 年度 2003
  • 页码 89 p.
  • 总页数 89
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 工程材料学;
  • 关键词

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