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Dynamic restoration mechanisms and microstructural refinement of alpha-zirconium with large strain deformation at elevated temperatures.

机译:在高温下具有大应变变形的α-锆的动态恢复机制和微观结构细化。

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摘要

The extensive use of zirconium as an elevated-temperature structural material in the nuclear industry since the 1950's has led to many investigations on its behavior during creep. A review of the different creep investigations of alpha zirconium is presented in the first part of this study. No agreement for the mechanism governing creep of zirconium was found among the different creep mechanisms considered for the relevant stress range. However, a review article recently showed that alpha-zirconium follows five-power law creep at intermediate modulus-compensated stress levels. This indicates that dislocation-climb is the deformation mechanism, with dynamic recovery as the restoration mechanism. This implies that the creep activation energy should be equal to the self-diffusion activation energy. However, the discrepancy between the published data of creep and self-diffusion activation energies suggests a different creep mechanism and/or an extra restoration mechanism could be occurring.; Constant strain-rate tensile and torsion and constant stress tests were performed between 400 and 800°C. Constant strain-rate torsion tests were utilized to calculate the variation of the activation energy with temperature. It appears that the apparent activation energy followed the same trend as the self-diffusion activation energy, suggesting dislocation climb as the rate-controlling mechanism and dynamic recovery as the restoration mechanism. The grain refinement observed during constant strain-rate tests was characterized by polarized optical microscopy, transmission electron microscopy and convergent beam electron diffraction, along with electron backscattered diffraction (EBSD). No evidence of discontinuous dynamic recrystallization was observed and dynamic recovery, via dislocation climb, appears to be the sole restoration mechanism. Also, it appears that the formation of small, equiaxed (sub)grains leading to a significant grain refinement and a bimodal distribution of boundary misorientation are due to geometric dynamic recrystallization. Texture analysis by X-ray diffraction and EBSD revealed that the softening observed above 650°C is likely caused by the development of a deformation texture. Finally, a study is proposed to assess the mechanism of formation of high-angle boundaries in single crystals. This could bring insights on the controversy regarding the existence of continuous dynamic recrystallization and help develop a reliable technique to study the evolution of high-angle boundaries with plastic deformation.
机译:自1950年代以来,锆在核工业中被广泛用作高温结构材料,这导致人们对其蠕变期间的行为进行了许多研究。本研究的第一部分介绍了对α锆的不同蠕变研究的综述。在针对相关应力范围考虑的不同蠕变机理中,未发现控制锆蠕变的机理。但是,最近的一篇评论文章显示,α-锆在中等模量补偿的应力水平下遵循五次幂定律蠕变。这表明位错上升是变形机制,而动态恢复是恢复机制。这意味着蠕变激活能应等于自扩散激活能。然而,蠕变和自扩散活化能的公开数据之间的差异表明,不同的蠕变机制和/或可能会发生额外的恢复机制。在400至800°C之间进行了恒定应变率拉伸和扭转以及恒定应力测试。恒定应变率扭转试验用于计算活化能随温度的变化。似乎表观活化能遵循与自扩散活化能相同的趋势,表明位错爬升是速率控制机制,动态恢复是恢复机制。在恒定应变率测试期间观察到的晶粒细化通过偏振光学显微镜,透射电子显微镜和会聚束电子衍射以及电子背散射衍射(EBSD)进行表征。没有观察到不连续的动态再结晶的证据,通过位错爬升的动态恢复似乎是唯一的恢复机制。同样,似乎导致几何显着细化的小等轴(亚)晶粒的形成导致明显的晶粒细化和边界取向错误的双峰分布。通过X射线衍射和EBSD进行的织构分析表明,在650°C以上观察到的软化可能是由变形织构的发展引起的。最后,提出了一项研究来评估单晶中高角度边界形成的机制。这可能会带来有关连续动态再结晶存在的争议的见解,并有助于开发一种可靠的技术来研究具有塑性变形的高角度边界的演化。

著录项

  • 作者

    Barrabes, Stephane R.;

  • 作者单位

    University of Southern California.;

  • 授予单位 University of Southern California.;
  • 学科 Engineering Mechanical.; Engineering Materials Science.
  • 学位 Ph.D.
  • 年度 2005
  • 页码 196 p.
  • 总页数 196
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 机械、仪表工业;工程材料学;
  • 关键词

  • 入库时间 2022-08-17 11:42:08

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